M. Salehi
Department of Chemistry, Faculty of Sciences, Semnan University, Semnan, I. R. Iran.
[ 1 ] - Novel Synthesis of Manganese Spinel Nanoparticles via Combustion with MnIII(acac)3 as Precursor
In the present work Mn3O4 nanoparticles (NPs) with spinel structure were synthesized successfully via combustion route with MnIII(acac)3 as precursor in two different temperatures. The morphology of the synthesized Mn3O4 were investigated by field emission scanning electron microscope (FESEM) and structural analysis was studied by po...
[ 2 ] - Hydrothermal Synthesis, Structural and Catalytic Studies of CuBi2O4 Nanoparticles
In the present work CuBi2O4 nano-spinel has been synthesized via mild hydrothermal methodat 180°C for 10 h. The synthesized nanomaterials were characterized by several techniquesto emphasis the structure and properties of produced materials. The crystal structure wasinvestigated by X-ray powder diffraction method and the values of the refined unit cell volumeand the structure properties were st...
[ 3 ] - New Method for Preparation of Nano Alumina Powder Using Aluminum(III) Complexes by Combustion Synthesis Without Fuel
Alumina nanomaterials were synthesized via a solution combustion technique using tris-(acetylacetonato) aluminum(III) complex (1) and tris-(2-formylphenolate) aluminum(III) complex (2) at 600, and 1000 °C for 3h. The obtained data showed that the procedure without using fuel resulted in a better phase and morphology. To investigate the phase formation, powder X-ray diffraction technique was use...
[ 4 ] - سنتز و شناسایی نانو کریستال اکسید کبالت دوپه شده بانئودیمیوم و یوروپیوم، مطالعه نانوذره سنتزی در واکنش تکاملی اکسیژن
در مطالعه حاضر، شناسایی نانوذرات Co3o4و دوپه نئودیمیوم و یوروپیوم روی کبالت اکسید ارائه شد. نانوذرات با استفاده از روش سنتز احتراقی، در دمای 700 درجه سانتیگراد و مدت 8 ساعت با استفاده از کمپلکسCo(acac)3 تهیه شدند. سپس، نانوذرات به وسیله طیف سنجی مادون قرمز (IR)، میکروسکوپ الکترونی روبشی نشر میدانی (FE-SEM)، طیف سنجی پراش اشعه ایکس (XRD)، اسپکتروسکوپی اشعه ایکس انرژی متفرق (EDS) و طیف سنجی...
[ 5 ] - اثر دما بر مورفولوژی، اندازه ذرات و خواص مغناطیسی نانو ذرات Co3O4 سنتز شده به روش احتراقی
کبالت اکسید در ابعاد نانو به روش سنتز احتراقی با استفاده از کمپلکس [Co(acac)3] به عنوان پیش ماده در دمای 600 و 800 درجه سانتیگراد سنتز شد. نانو ذرات سنتز شده در این دو دما توسط میکروسکوپ الکترونی روبشی (FESEM)، پراش اشعه ایکس (XRD)، FTIR و VSM شناسایی و آنالیز شد. اثر دما بر روی اندازه ذرات، مورفولوژی و خاصیت مغناطیسی این نانو ذرات مورد بحث قرار گرفت. نتایج آنالیز میکروسکوپ الکترونی روبشی نش...
[ 6 ] - روش جدید برای تهیه پودرهای زیر میکرون کرم اکسید (III) توسط روش حالت جامد بدون استفاده از سوخت
یک روش حالت جامد برای سنت پودرهای زیر میکرون Cr2O3 با استفاده از [CrIII(acac)3] توسط روش سوزاندن بدون استفاده از سوخت گزارش شد. تکنیک پراش اشعه ایکس برای بررسی تشکیل فاز استفاده شد. همچنین میگروگراف های FESEM برای بررسی مورفولوژی مواد بدست آمده استفاده شدند. این نشان داد که مورفولوژی مواد بدست آمده در شکل مواد متخلخل و مواد با اندازه نانو بود. ویژگی های نوری مواد بدست آمده توسط طیف های FTIR مط...
[ 7 ] - Structural, magnetic and electrical properties of pure and Dy-doped Fe2O3 nanostructures synthesized using chemical thermal decomposition technique
Pure (S1) and Dy3+-doped α-Fe2O3 (S2 and S3) nanoparticles were prepared by a combustion synthesis method at 700 ºC for 8 h using Fe(acac)3 (Tris(acetylacetonato)Iron(III)) as raw material. Characterizations of the prepared powders were carried out by powder X-ray diffraction (PXRD). Structural analysis was performed b...
[ 8 ] - Solid state synthesis of MgAl2O4 nanomaterials and solar light-induced photocatalytic removal of Malachite Green
Spinel MgAl2O4 nanopowders were synthesized by one-step solid state reactions using Al(NO3)3.9H2O and MgSO4 raw materials at stoichiometric 1 : 2, Mg : Al molar ratio at a constant reaction temperature of 1000 ºC for 8 h (S1), 10 h (S2) and 24 h (S3). The synthesized materials were characterized...
[ 9 ] - Structural, magnetic and dielectric properties of pure and Dy-doped Co3O4 nanostructures for the electrochemical evolution of oxygen in alkaline media
In this study, spinel-type cobalt oxide (Co3O4) and Co3-xDyxO4 (x = 0.04 and 0.05 molar ratio) nanoparticles were synthesized via combustion method at 700 °C. Crystallite nature, phase purity and thermal analysis of the prepared compounds were investigated by PXRD, FT-IR and TGA techniques. Structural analyses were performed by the FullProf program employing profile matching with constant scale...
[ 10 ] - Synthesis and characterization of new spinel Mn0.5Cu0.5Cr2O4 and degradation of Malachite Green from wastewater in comparison with CuCr2O4
In this study phase- pure new spinel structure, Mn0.5Cu0.5Cr2O4 was prepared by hydrothermal method successfully and the degradation of Malachite green as an organic pollutant was investigated and compared with CuCr2O4. Purification of obtained nanoparticles was measured by using X-ray diffraction method (XRD) in which crystal st...
[ 11 ] - Solid state synthesis of MgAl2O4 nanomaterials and solar light-induced photocatalytic removal of Malachite Green
Spinel MgAl2O4 nanopowders were synthesized by one-step solid state reactions using Al(NO3)3.9H2O and MgSO4 raw materials at stoichiometric 1 : 2, Mg : Al molar ratio at a constant reaction temperature of 1000 ºC for 8 h (S1), 10 h (S2) and 24 h (S3). The synthesized materials were characterized...
[ 12 ] - Structural, magnetic and electrical properties of pure and Dy-doped Fe2O3 nanostructures synthesized using chemical thermal decomposition technique
Pure (S1) and Dy3+-doped α-Fe2O3 (S2 and S3) nanoparticles were prepared by a combustion synthesis method at 700 ºC for 8 h using Fe(acac)3 (Tris(acetylacetonato)Iron(III)) as raw material. Characterizations of the prepared powders were carried out by powder X-ray diffraction (PXRD). Structural analysis was performed b...
[ 13 ] - Synthesis and Characterization of Ni0.5Cu0.5Cr2O4 Nanostructure for Discoloration of Aniline Dye under Visible Light from Wastewater
In this research, pure-phased Ni0.5Cu0.5Cr2O4 synthesis via solid-state method successfully. In the other part, the photocatalytic activity of synthesized Ni0.5Cu0.5Cr2O4 was investigated in various aspects by using Malachite green as a pollutant and compared with the number of previous photocatalysts. T...
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