Michal Dusek
Institute of Physic of the Czech Academy of Sciences, Na Slovance 2, 182 21 Prague 8, Czech Republic
[ 1 ] - New 16-membered macrocyclic Schiff base: Synthesis, structural and FT-IR studies
In this paper, the structure of a new 16-membered macrocyclic Schiff base compound N,N′-(3,3′-dimethoxy-2,2′-(propane-1,3-diyldioxy)dibenzylidene)propane-1,3-diamine, C22H26N2O4 (1), derived from 1,3-propanediamine and 3,3′-dimethoxy-2,2′-(propane-1,3-diyldioxy)dibenzaldehyde has been studied by single crystal X-ray diffraction, DFT calculations at B3LYP/6-31G** and FT-IR spectroscopy. The titl...
[ 2 ] - Nickel(II) and Copper(II) Complexes of a New Tetradentate Schiff Base Ligand: Synthesis, Characterization, Thermal Studies and Use as Precursors for Preparation of NiO and CuO Nanoparticles
A new tetradentate N2O2 Schiff base ligand (MeO-bph)2bn = N,N¢-bis(2-hydroxy-4-methoxybenzophenone)-1,4-butanediamine was prepared from the condensation of butane-1,4-diamine with 4-methoxy-2-hydroxybenzophenone and characterized by 1H-NMR spectroscopy and single-crystal X-ray diffraction. Its nickel(II) and copper(II) complexes characterized usin...
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