For the determination of adenosine-5’-phosphoric acid and its homologues the methods which have been recommended chiefly are (1) enzymatic deamination by deaminase and quantitative determination of the ammonia split off (1) ; (2) determination on the basis of the pharmacological activity, (a) contraction of the isolated guinea pig uterus, (b) the characteristic change in the electrocardiogram u...

The aim of this study was to determine whether there was any difference in the degree of enamel loss at bond-up, debond and enamel clean-up when two different adhesive systems were tested and with four different methods of enamel clean-up. The adhesive systems were 37 per cent o-phosphoric acid with Transbond XT (group 1) and 10 per cent poly(acrylic acid) conditioner with Fuji Ortho LC (group ...

BACKGROUND Molar bonding procedures need continuous improvement to be widely accepted clinically and eventually replace molar bands. MATERIAL AND METHODS The purpose of this study was to determine the effects of enamel micro-abrasion and silane coating of the base of molar tubes on shear and tensile bond strengths of orthodontic molar tubes. A total of 200 third molars were randomly allocated...

Two high-performance liquid chromatography (HPLC) methods for ascorbic acid (AA) quantification were compared in three cultivars of melon (Cucumis melo L.) fruits. Both procedures were analogous except for the extraction medium used: 6 % meta-phosphoric acid and 3 % citric acid. The general conclusion is that 3 % citric acid is a better extraction medium compared to 6 % meta-phosphoric acid and...

OBJECTIVES This study evaluated the effect of etching using 2% proanthocynidin-containing 10% phosphoric acid 2% PA/10% PhA vs. 35% phosphoric acid 35% PhA on immediate (IM) and 6-months (6M) resin-enamel microshear bond strength (μSBS), resin-dentin microtensile bond strength (μTBS), nanoleakage (NL) and as well as in situ MMP inhibition potential. METHODS The dentin surface of human were ex...

AIM The purpose of this study was to assess the effect of different surface treatments on the shear bond strength (SBS) of a resin modified glass ionomer cement (RMGIC) to dentin. METHODS AND MATERIALS Forty human third molar teeth were randomly divided into four groups (n=10). The occlusal enamel was removed to obtain a flat surface of dentin. Each group was treated as follows: Group 1: 10% ...

The objective of this study was to evaluate the effectiveness of a self-etching primer, Transbond Plus Self Etching Primer (TSEP, 3M Unitek), and a non-rinse conditioner (NRC, Dentsply DeTrey) for bonding brackets, compared with the acid-etch technique. The brackets were bonded to extracted premolars using Transbond XT (3M Unitek). One of the following three conditioning protocols were used: (1...

Key words iridium catalysis - chiral phosphoric acid photocatalyst 2+2 cycloaddition