نتایج جستجو برای: by transition electron microscope tem various factors influencing

تعداد نتایج: 8064543  

Plant-mediated synthesis of metal oxide nanoparticles is a promising alternative to the traditional method of physical and chemical synthesis. In this paper, we report the green synthesis of zinc oxide nanoparticles (ZnONPs) by a biological method. During the study, Zinc oxide nanoparticles were synthesized by Allium sativum skin (garlic skin) extract. Formation of zinc oxide nanoparticles has ...

2014
Felix Börrnert Thomas Riedel Heiko Müller Martin Linck Bernd Büchner Hannes Lichte

The progress in (scanning) transmission electron microscopy has led to an unprecedented knowledge of the microscopic structure of functional materials at the atomic level. Additionally, although not widely used yet, electron holography is capable to map the electric and magnetic potential distributions at the sub-nanometer scale. Nevertheless, in-situ studies inside a (scanning) transmission el...

Journal: :Ultramicroscopy 2006
Gian Carlo Capitani Peter Oleynikov Sven Hovmöller Marcello Mellini

A practical, offline method for experimental detection and correction for projector lens distortion in the transmission electron microscope (TEM) operating in high-resolution (HR) and selected area electron diffraction (SAED) modes is described. Typical TEM works show that, in the simplest case, the distortion transforms on the recording device, which would be a circle into an ellipse. The firs...

FePt nanoparticles with thermally stable room-temperature ferromagnetism are investigated. The monodisperse nanoparticles are prepared by chemical synthesis and a salt-matrix annealing technique. Structural and magnetic characterizations confirm the phase transition from the disordered face-centered cubic structure. In this paper, 3 nm FePt nanoparticles are first synthesized by superhydride re...

Journal: :Philosophical transactions. Series A, Mathematical, physical, and engineering sciences 2009
S J Haigh H Sawada Angus I Kirkland

Transmission electron microscope (TEM) images recorded under tilted illumination conditions transfer higher spatial frequencies than axial images. This super resolution information transfer is highly directional in a single image, but can be extended in all directions through the use of complementary beam tilts during exit wave function reconstruction. We have determined the optimal experimenta...

S. Sadegh Hassani, Z. Sobat

The Scanning Probe Microscopes (SPMs) based lithographic techniques have been demonstrated as an extremely capable patterning tool. Manipulating surfaces, creating atomic assembly, fabricating chemical patterns, imaging topography and characterizing various mechanical properties of materials in nanometer regime are enabled by this technique. In this paper, a qualified overview of diverse lithog...

2017
Sapana S. Madan Kailas L. Wasewar

Nanoparticles of CaO2 were synthesized by chemical precipitation method and characterized by X-ray powder diffraction (XRD), scanning electron microscope (HR-FESEM), energy-dispersive X-ray spectroscopy (EDX), transmittance electron microscopy (TEM) and high-resolution TEM (HRTEM). HR-FESEM, TEM, and HRTEM images confirmed the average size of nanoparticles as 10–40 nm. Furthermore, application ...

2010
Binghui Wang Xupin Zhuang Wenjian Deng Bowen Cheng

Silver nanoparticles were prepared by microwave irradiation of silver nitrate solution with carboxymethyl chitosan as reducing agent and a stabilizer. The optical properties, morphology and structure were characterized using UV–Visible spectrophotometer, transmission electron microscope (TEM) and X-ray diffraction (XRD). Appearance of surface plasmon band at 413 nm indicated the formation of si...

In this paper, the magnetic properties of carbon based material, graphene is studied, which is generated by laser ablation in cryogenic media. Transmission electron microscopy (TEM) and alternating gradient force magnetometer (AGFM) are applied to investigate the graphene morphology and magnetic properties, respectively. The graphene synthesized by the laser ablation method exhibits diamagnetic...

2001
Steven J Ludtke Wah Chiu

The transmission electron microscope (TEM) is a versatile device used in fields ranging from material science to cell biology to biochemistry. In a light microscope, the light wavelength is typically about 5000 Å, which makes it the primary resolution-limiting factor. In aTEM,however, the electron wavelength is typically less than 0.04 Å, much smaller than the size of a single atom. The resolut...

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