A gas chromatography-mass spectrometry (GC-MS) method was validated for the determination of 16 polycyclic aromatic hydrocarbons (PAHs) from the FDA list of 93 harmful or potentially harmful constituents of mainstream cigarette smoke (MCS). Target analytes were extracted from total particulate matter using accelerated solvent extraction with a toluene/ethanol solvent mixture. Matrix artefacts w...

Identifying non-annotated peaks may have a significant impact on the understanding of biological systems. In silico methodologies have focused on ESI LC/MS/MS for identifying non-annotated MS peaks. In this study, we employed in silico methodology to develop an Isotopic Ratio Outlier Analysis (IROA) workflow using enhanced mass spectrometric data acquired with the ultra-high resolution GC-Orbit...

Gas chromatography mass spectrometry (GC-MS) is a widely used central analytical technology. Commercially available GC-MS systems use different types of mass analyzers such as Quadrupole, Ion Trap and/or Time of Flight, but practically all systems utilize the same Nier type electron ionization (EI) ion source and the same standard GC-MS transfer-line interface. Consequently, the various GC-MS v...

background & aim: elaeagnus angustifolia and elaeagnus orientalis have a lot of medical utilization. in folk medicine, the fruit and flower of these plants are used as a tonic and antipyretic agent. the aim of the present study was to chemical analysis of volatile constituents of e. angustifolia and e. orientalis flowers.  experimental: the essential oils of e. angustifolia and e. orientali...

background & aim: saline lands can be utilized by planting native medicinal plants tolerant to salinity. the quantity and quality these plants are changed during various seasons in agriculture systems. thus, this study carried out under salinity stress in order to examine the effect of sowing in two seasons on growth characteristics and essential oil  components of ajowan (carum capticum l....

in this experiment, the chemical composition of the essential oils obtained from ferula assa-foetida oleo-gum resin collected from two different sites of yazd province (tabas and yazd) in the center of iran, were identified. the gas chromatography mass-spectroscopy (gc/ms) data showed that the qualitative composition of the components appeared to be constant in two different regions. moreover, ...

background and objectives: several natural compounds have been identified for the treatment ofleishmaniasis. due to a few safe drugs and the side effects caused by available chemotherapy, some new drugs for treatment of leishmaniasis are requested.  the genus pulicaria (asteraceae) is represented in the flora of iran by five species. phytochemical studies on pulicaria species have revealed some...

dibutyl phthalate (dbp) is a phthalic acid ester and is widely used in polymeric products to make them more flexible. dbp is found in almost every plastic material and is believed to be persistent in the environment. various analytical methods have been used to measure dbp in different matrices. considering the ubiquitous nature of dbp, the most important challenge in dbp analyses is the contam...

cucumber is one of the main vegetables in iranian food basket. a wide range of pesticides are used for crops protection during the cultivation of vegetables such as cucumber due to heavy pest infestation. analysis of pesticide residues in food and other environmental commodities have become essential requirement for consumers, producers, and food quality control authorities. this study was aime...

the chemical composition of the hydrolate of citrus aurantium l. (rutaceae) flowers (neroli) grown in iran, and two commercial hydrolates were analyzed by gc/ms. thirty compounds (90.3%) were identified in the hydrolate by the use of laboratory apparatus, thirty-eight compounds (83.4%) in the hydrolate from the traditional method and fifteen compounds (98.3%) in the industrially produced sample...