نتایج جستجو برای: gc fid

تعداد نتایج: 36940  

Journal: :Analytical and bioanalytical chemistry 2008
Michele M Schantz Mary Bedner Stephen E Long John L Molloy Karen E Murphy Barbara J Porter Karsten Putzbach Catherine A Rimmer Lane C Sander Katherine E Sharpless Jeanice B Thomas Stephen A Wise Laura J Wood James H Yen Takashi Yarita Agnes NguyenPho Wendy R Sorenson Joseph M Betz

As part of a collaboration with the National Institutes of Health's Office of Dietary Supplements and the Food and Drug Administration's Center for Drug Evaluation and Research, the National Institute of Standards and Technology has developed two standard reference materials (SRMs) representing different forms of saw palmetto (Serenoa repens), SRM 3250 Serenoa repens fruit and SRM 3251 Serenoa ...

Journal: :Natural Volatiles and Essential Oils 2021

The essential oil composition from the leaves of Strychnos axillaris Colebr. (Loganiaceae) growing in Malaysia was examined for first time. obtained by hydrodistillation and fully characterized gas chromatography (GC-FID) chromatography-mass spectrometry (GC-MS). In total, 15 components were identified oil, which made up 87.2% total oil. is composed mainly ?-ionone (20.2%), ?-ionone (19.5%), bi...

Journal: :Biomedical chromatography : BMC 2015
Mirela Rada José María Castellano Javier S Perona Ángeles Guinda

Analytical interest of OA determination in human serum has increased owing to the increasing interest in pharmaceutical research by pharmaceutical properties. A simple, specific, precise and accurate GC method with flame ionization detector (FID) developed and validated for the determination of oleanolic acid (OA) in human serum (HS). To an aliquot of HS, internal standard was added and a combi...

2002
Luigi Mondello Philip Marriott Giovanni Dugo

Nine samples of lavender essential oil were analysed by GC–MS using low-polarity and polar capillary columns. Linear retention indices (LRI) were calculated for each component detected. Characterisation of the individual components making up the oils was performed with the use of an mass spectrometry (MS) library developed in-house. The MS library was designed to incorporate the chromatographic...

Journal: :Molecules 2010
Hong-Wu Wang Yan-Qing Liu Shou-Lian Wei Zi-Jun Yan Kuan Lu

Microwave-assisted hydrodistillation (MAHD) is an advanced hydrodistillation (HD) technique, in which a microwave oven is used in the extraction process. MAHD and HD methods have been compared and evaluated for their effectiveness in the isolation of essential oils from fresh mango (Mangifera indica L.) flowers. MAHD offers important advantages over HD in terms of energy savings and extraction ...

2015
Á. Calín-Sanchez F. Hernandez P. Melgarejo P. Legua

Commercial juices of sweet pomegranates and fresh juices of sour-sweet pomegranates were analysed for organic acids, sugars, antioxidant activity, volatile composition, sensory profile and consumer liking. Organic acids and sugars were analysed by HPLC, while volatiles were extracted using hydrodistillation and analysed by GC-MS and GC-FID. Malic acid was predominant in sweet juices while citri...

2009
Oscar S. GIORDANO Marta E. SOSA

„ Toxic and repellent properties of whole essential oils from four Eupatorium (Asteraceae) species (E. buniifolium Hook. et Arn, E. inulaefolium Kunth, E. arnottii Baker, and E. viscidum Hook. & Arn) were investigated in different concentrations toward Tribolium castaneum Herbst adults. The essential oils were isolated by hydrodistillation techniques from the aerial parts. The analysis was perf...

2011
Mohammad Sharif Sharifi Stuart Loyd Hazell

The volatile oil from the crude gum of Kurdica, from Pistacia atlantica Kurdica, was isolated by hydrodistillation and analyzed through a combination of gas chromatography (GC-FID) and gas chromatography/mass spectrometry (GC-MS). The essential oil formed 20% of the weight of the crude gum. The major constituent was α-Pinene. The extracted essential oil was then screened for antimicrobial activ...

2010
Morteza Akramian Javad Hadian Mohammad Reza Joharchi Behvar Asghari Hasan Mumivand

The oil obtained by hydrodistillation of aerial parts of Phlomis elliptica Benth. (Labiatae), which is a rare shrub endemic to Iran, was subjected to GC-FID and GC-MS analyses. Thirty-one constituents, making up about 98.4 % of the total composition of oil, were characterized. Monoterpenes, sesquiterpenes and other compounds constituted 13.4 %, 78.9 % and 6.1 % of the essential oil, respectivel...

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