This paper reports an investigation of the microwave-assisted synthesis of silver nanoparticles (Ag NPs) using extract of stinky bean (Parkia speciosa Hassk) pods (BP). The formation of Ag NPs was identified by instrumental analysis consists of UV-vis spectrophotometry, Fourier-transform infrared (FTIR) spectrophotometry, scanning electron microscopy (SEM), transmission electron microscopy (TEM...

This study investigated how the inclusion of magnesium oxide (MgO) maintained tablet hardness during storage in an unpackaged state. Tablets were prepared with a range of MgO levels and stored at 40°C with 75% relative humidity for up to 14 d. The hardness of tablets prepared without MgO decreased over time. The amount of added MgO was positively associated with tablet hardness and mass from an...

The title reaction was studied by photolyzing mixtures of CI2 and SO2 with and without 02 present in an atmosphere of N2, using Fourier transform infrared spectrophotometry to monitor reactants and products. In the absence of oxygen, sulfur dioxide is quantitatively converted to sulfuryl chloride. With 10 to 150 Torr 02 present H2SO4 is produced as well as SO2C12. When a number of speculative r...

The aim is to study cerebral vascular functional connectivity during motor tasks and resting state using multichannel frequency-domain near-infrared spectrophotometry. Maps of 5.7 × 10.8 cm size displaying changes in cerebral oxyhemoglobin (O(2)Hb), deoxyhemoglobin (HHb), and total hemoglobin (tHb) concentrations were measured in the motor cortex in 12 subjects (mean age of 28.8±12.7 yrs) durin...

In studies of intestinal absorption non-absorbed markers are used to indicate changes in volume of the contents of the bowel. Polyethylene glycol 4000 (PEG 4000), a popular marker, has been shown to fulfil the criteria of a volume indicator (Hyden, 1956b; Jacobson, Bondy, Broitman, and Fordtran, 1963; Maddrey, Serebro, Marcus, and Iber, 1967; Shields, Harris, and Davies, 1968). The concentratio...

With the use of a high-resolution grating infrared spectrophotometer, it is possible to analyze mixtures of cholesterol esters and triglycerides on the basis of the difference in their ester carbonyl absorption frequencies. In the analysis of serum lipids, the preliminary removal of phospholipids is accomplished by a simple batch adsorption on silicic acid. Infrared absorbance measurements are ...

Extension of optical monitoring of intact tissues from the visible and ultraviolet to the near-infrared (NIR) range (700-1300 nm) was first undertaken in 1977 for the purpose of monitoring the redox behavior of Cytochrome c oxidase (cyt c ox) in vivo. Soon it became evident that the much greater NIR translucency of skin and bone made it possible to reach brain and muscle tissue without surgical...

It is not known whether microcalculi possess structural differences compared with larger stones or whether they represent simply an earlier stage in stone disease. We carried out a controlled study on 10 patients affected by gallbladder cholesterol microlithiasis (CM). In all patients, samples from all parts of the stones were studied by X-ray diffraction and by infrared spectrophotometry. Bile...