most areas of plain regions in mazandaran province are planted with rice, and different pesticides and fertilizers are used at high densities to increase the yield of production. diazinon is the main insecticide that being used to control chilo supressalis walker. the main problem is the high groundwater table in the region, and consumption of this water by local people and anthropogenic side e...

A simple high-performance liquid chromatographic method with ultraviolet detection is proposed for the estimation of diclofenac potassium and drotaverine hydrochloride in human plasma. Liquid-liquid extraction was carried out with a mixture of dichloromethane-isopropyl alcohol (80:20, v/v). Chromatographic separation of the analytes and internal standard was achieved on an analytical 250 × 4.6 ...

A rigours mathematical model based on the bivariate population balance frame work (the base of LLECMOD ‘‘Liquid-Liquid Extraction Column Module’’) for the steady state and dynamic simulation of pulsed liquid-liquid extraction columns is developed. The model simulates the coupled hydrodynamic and mass transfer for pulsed (packed and sieve plate) extraction columns. It is implemented using visual...

When the free cortisol in urine was analyzed by liquid chromatography after pretreatment with the usual organic extraction, interfering substances having chromatographic behavior similar to that of cortisol and the internal standard precluded accurate measurement. To remove these materials, we processed the organic extract by liquid chromatography with a normal-phase column for clean-up; the sp...

A validated HPLC method was developed to determine the doxorubicin concentration in a small volume of rat plasma (60 µL) with convenient fluorescence detection. Sample preparation includes a simple one-step liquid-liquid extraction using a minimum amount of organic solvent, with extraction recovery more than 95%. The analysis was accomplished using PerfectSil C18 column maintained at 35 °C and ...

a simple and reproducible hplc method with spectrophotometric detection was developed for determination of rivastigmine in human plasma. liquid-liquid extraction of rivastigmine and donepezil (as internal standard) from plasma samples was performed with 1-butanol/n-hexane (2:98 v/v) in alkaline condition followed by back-extraction into diluted acetic acid. chromatography was carried out using ...

in this project, eggshell membrane was used as a solid phase extraction sorbent for extraction of morphine followed by hplc analysis. at first, raw eggshell membrane was used and then, because of low adsorption of morphine on untreated eggshell membrane (

Extraction and determination of naproxen from human plasma were performed using Vortex-Assisted Inverted Dispersive Liquid-Liquid MicroExtraction (VA−IDLLME) and High-Performance Liquid Chromatography (HPLC). The parameters affecting extraction recovery such as type and volume of extraction and disperser solvents, pH of sample solution, stirring rate, extraction time and salt addition were ...

The tuned liquid column damper (TLCD) having a uniform cross-sectional tube of U-shaped, occupied with liquid is used as a vibrational response mitigation device. The tuned liquid column ball damper (TLCBD) is a modified TLCD, where, an immovable orifice, positioned at the middle part of the horizontal portion, is replaced by a metal ball. Different studies on the unconstrained optimization per...