H and C nuclear magnetic resonance (NMR) spectra were recorded at 400 MHz on a Bruker ARX-400 NMR spectrometer (Germany) with tetramethylsilane as internal standard. Column chromatography was performed using Merck (Germany) silica gel (230-400 mesh). Thin layer chromatography (TLC) was performed using Merck silica gel GF254, 0.25 mm thickness. For visualization, TLC plates were placed under aci...

Quantum tunneling frequencies of methyl groups at low temperature can be measured directly by low-field nuclear magnetic resonance (NMR) using our d&QUID (superconducting quantum interference device) spectrometer. From NMR spectra recorded in magnetic fields below 20 mT, tunneling frequencies between I40 and 250 kHz were measured for a homologous series of carboxylic acids at 4.2 K. For solids ...

Purpose: To assess the relationship between the severity of coronary arteries involvement and the extent and pattern of myocardial scars in Cardiac Magnetic Resonance of patients with history of remote myocardial infarction. Materials and Methods: The Cardiac Magnetic Resonance images of sixty patients with history of remote ST segment or non-ST segment elevation myocardial infarction were ...

The effects of chemotherapy on living tumor tissue in hamsters and rats were investigated by measuring the 31P nuclear magnetic resonance spectra using topical magnetic resonance. Human neuroblastoma, human glioblastoma, and rat glioma tumor cells were inoculated s.c. in the lumbar region of the animals. After the diameter of the tumors increased to 1.5 cm, in vivo 31P nuclear magnetic resonanc...

In the present work, a new method for measuring motional parameters using the off-resonance technique was described. The Lipari-Szabo model-free formalism was used to analyze molecular dynamics in a heteronuclear system [1, 2]. Cross-relaxation solid state nuclear magnetic resonance off-resonance experiments were performed on a homebuilt pulse spectrometer operating at the frequency of 30.2 MHz...