Nanocrystalline alumina powder has been synthesized using solution combustion method. The obtained nanocrystalline alumina powder was used as an efficient catalyst for the synthesis of imidazo[1,2-a]azine derivatives from one-pot three component reaction of benzaldehyde, 2-aminoazine and trimethylsilylcyanide under ultrasonic irradiation and refluxing condition. Reusability of catalyst and shor...

nanocrystalline alumina powder has been synthesized using solution combustion method. the obtained nanocrystalline alumina powder was used as an efficient catalyst for the synthesis of imidazo[1,2-a]azine derivatives from one-pot three component reaction of benzaldehyde, 2-aminoazine and trimethylsilylcyanide under ultrasonic irradiation and refluxing condition. reusability of catalyst and shor...

Citation: Potemkin DI, Maslov DK, Loponov K, Snytnikov PV, Shubin YV, Plyusnin PE, Svintsitskiy DA, Sobyanin VA and Lapkin AA (2018) Porous Nanocrystalline Silicon Supported Bimetallic Pd-Au Catalysts: Preparation, Characterization, and Direct Hydrogen Peroxide Synthesis. Front. Chem. 6:85. doi: 10.3389/fchem.2018.00085 Porous Nanocrystalline Silicon Supported Bimetallic Pd-Au Catalysts: Prepar...

In this study, the removal of cadmium and lead ions from aqueous solution by nanocrystalline magnetite was investigated. The nanocrystalline magnetite was synthesized by mechanochemical activation of hematite in a high energy planetary mill in argon atmosphere for 45 hours. The ability of the synthesized nanocrystalline magnetite for removal of Cd(II) and Pb(II) from aqueous solutions was studi...

Nanocrystals and nanoclusters of the room-temperature magnetic spinel CuCr(2)S(4) have been synthesized using a facile solution-based method. The synthesis involves hot injection of an excess of 1-dodecanethiol (1-DDT) into a boiling coordinating solvent containing CuCl(2) and CrCl(3)·6H(2)O. Using octadecylamine (ODA) as a solvent yields cube-shaped nanocrystals with an average size of 20 ± 2 ...

the mechanical properties and microstructural developments of 321 stainless steel during thermomechanicalprocess were investigated. the repetitive cold rolling and subsequent annealing wereconducted to achieve nanocrystalline structure in an aisi 321 stainless steel. heavily cold rolling at−20°c was conducted to form martensite in metastable austenitic steel. the process was followed byannealin...

Nanocrystalline materials show a higher strain-rate sensitivity in contrast to the conventional coarse-grained materials and a different grain size dependency. To explain these phenomenon, a finite element model is constructed that considers both grain interior and grain boundary deformation of nanocrystalline materials. The model consist of several crystalline cores with different orientations...

A lower limit for the grain size of nanocrystalline solids obtained by crystallization of the glass and its dependency on the crystallization temperature are thermodynamically considered. It is found that the nanocrystalline materials have the smallest grain size when the crystallization temperature is roughly half of the melting temperature. At this temperature, the Gibbs free energy differenc...

nanocrystalline ceria has been considered as support for carbon monoxide preferentially oxidation. in this study ceria was prepared by precipitation method and the effects of preparation conditions, such as ph of solution (8-10), aging time (1-12 hr), drying temperature (80-120 °c), calcination time (2-6 hr) and temperature (400-600 °c) were investigated on ceria synthesized powders properties....