نتایج جستجو برای: ray diffraction and micro
تعداد نتایج: 16903940 فیلتر نتایج به سال:
Current analytical techniques for characterizing solid-state pharmaceuticals include powder x-ray diffraction, differential scanning calorimetry, thermogravimetric analysis, infrared spectroscopy, Raman spectroscopy, electron microscopy and nuclear magnetic resonance. Powder x-ray diffraction and differential scanning calorimetry are mainstream techniques but they lack spatial resolution. Scann...
In the synthesis of hexamethylenetetranitramine (HMX) by Bachmann method, the morphology of crude HMX products are needle-like with alpha polymorph. This quality of materials leads to separation of α-HMX from final suspension to be time-consuming and difficult. On the other hands, crude product of α-HMX are the more sensitive and unsafe than β-HMX. Herein, a seeding strategy wa...
Bulk single crystals of pure and xylenol orange dye (XO) admixtured L-Alanine Thiourea (LATU) were grown by slow evaporation technique. The cell parameters and crystallinity of pure and dye admixtured LATU crystals were confirmed by single crystal, powder X-ray diffraction and high resolution X-ray diffraction analyses. The functional groups present in the crystals were confirmed by FTIR analys...
Interaction with water causes shrinkage and significant changes in the structure of spider dragline silks, which has been referred to as supercontraction in the literature. Preferred orientation or alignment of protein chains with respect to the fiber axis is extensively changed during this supercontraction process. Synchrotron x-ray micro-fiber diffraction experiments have been performed on Ne...
For the very first time, atomic force microscope images of lamellar phases were observed combined with a freeze fracture technique that does not involve the use of replicas. Samples are rapidly frozen, fractured, and scanned directly with atomic force microscopy, at liquid nitrogen temperature and in high vacuum. This procedure can be used to investigate micro-structured liquids. The lamellar p...
The corrosion behavior of oxygen-free copper in anoxic sulfide solutions under nuclear waste disposal conditions was studied using electrochemical impedance spectroscopy (EIS), scanning electron microscopy (SEM) equipped with a focused ion beam (FIB), X-ray photoelectron spectroscopy (XPS) and Micro X-ray diffraction ( XRD). The film growth process and mechanism were elucidated using an Au mark...
Samarium-doped ZnO hierarchical micro/nanospheres (Sm/ZnO) were synthesized via a facile and surfactant-free chemical solution route. The obtained products were characterized by field-emission scanning electron microscopy (FESEM), transmission electron microscopy (TEM), X-ray diffraction (XRD), energy dispersive X-ray (EDX), UV–visible diffuse reflectance spectroscopy (UV-vis DRS) and photolumi...
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