The effects of anomalous dispersion (resonance) on multiple reflection of x rays and their interference in crystals at atomic absorption edges are studied. Intensity ratios of two inversion-symmetry-related multiple diffractions at or near absorption edges exhibit highly phase-sensitive profiles with strong asymmetric characteristics, unlike those far from the edges. A new resonance perturbatio...

The new complex of [H2en][Cu(pydc)2].2H2O (1) (where H2en and pydc are ethylenediammonium and 2,6-pyridinedicarboxylate, respectively) was synthesized by the reaction of a mixture of ethylenediamine (en) and 2,6-pyridinedicarboxylic acid (H2pydc) in a mixture of CH3OH/H2O as solvent. This complex was fully characterized by elemental analysis, IR, UV–Vis spectroscopy as well as single-crystal X-...

in this paper, we report on the synthesis of cu nanoparticles through a single-precursor route by controlling the growth temperature. selective adsorption of oleylamine on various crystal planes may play an important role in the growth process. the understanding of this self-assembling process will help us develop reliable and reproducible methods to synthesis other three dimensional nanostruct...

Recently, very thin single crystal scintillator imaging plates became of great interest. Such thin screens are mainly used in micro-CT and nano-CT systems with either micro-focus X-ray tubes or with synchrotron sources. This work deals with a high resolution CCD camera in conjunction with a macro optical system and YAG:Ce single crystal scintillators for low energy X-ray micro-radiography appli...

two new nano-sized lead(ii) and mercury(ii) coordination polymers, [pb(2-bpdh)(no3)2(h2o)]n(1); (2-bpdh = 2,5-bis(2-pyridyl)-3,4-diaza-2,4-hexadiene)} and [hg(4-bpdb)(scn)2]n (2); (4-bpdb= 1,4-bis(4-pyridyl)-3,4-diaza-1,3-butadiene) were synthesized by a sonochemical method. the structure of 1 may be considered coordination polymer of lead(ii) and single crystal x–ray analysis of compound 2reve...