phytoremediation has gained increasing attention in recent years because of its ability to clean up and redevelop brownfield sites. petroleum hydrocarbon-contaminated sites are among most prevalent industrial sites in iran as one of the top oil producers in the world, which are in great need of remediation to prevent associated environmental and human health risks. a greenhouse study was conduc...

A simple procedure was developed for in vitro synthesis and characterization of aflatoxin B1-lysine adduct using aflatoxin B1, N-alpha-acetyl lysine and m-chloroperbenzoic acid (MCPBA). At a molar ratio of 1:16 (aflatoxin B1:N-alpha-cetyl lysine), the recovery of adduct was 62%. Analysis of the adduct by thin-layer chromatography showed a single spot (Rf = 0). Absorption spectra of the adduct s...

BACKGROUND The kallikrein family is a group of 15 serine protease genes clustered on chromosome 19q13.4. Human kallikrein gene 13 (KLK13) is a member of this family and encodes for a trypsin-like, secreted serine protease (hK13). Given that other kallikreins are sequestered by serum protease inhibitors, we hypothesized that hK13 may also interact with similar inhibitors. Our objective was to id...

urinary 1-hydroxypyrene is frequently used as a major metabolite and biological indicator of the overall exposure to polycyclic aromatic hydrocarbons. in this study, solid phase extraction was appropriately conditioned with regard to sample ph, sample concentration, loading flow rate, elution solvent, washing solvent, sample volume and sorbent mass. octadecyl silica cartridge (c18) was used as ...

In this work, two approaches based on Dispersive Liquid-Liquid MicroExtraction (DLLME) and Dispersive Liquid-Liquid MicroExtraction based on Solidification of Floating Organic Drop (DLLME-SFO) were compared for the extraction and preconcentration of crocin from saffron and biological samples. Different DLLME and DLLME-SFO parameters influencing the extraction efficiency were studied and opt...

A capillary electrophoresis method was used for assay of some degradation products of carvedilol. The optimized parameters were as; running buffer 80 mM acetate dissolved in methanol/ethanol mixture (65:35 v/v), applied voltage of 19 kV, temperature is 20 ºC and the wavelength range of 200-350 nm. The results indicate that the proposed CE method could effectively separate carvedilol from its de...

A complete variational treatment is provided for a family of spiked-harmonic oscillator Hamiltonians H = − d dx2 + Bx + λ x (B > 0, λ > 0 ), for arbitrary α > 0 . A compact topological proof is presented that the set S = {ψn} of known exact solutions for α = 2 constitutes an orthonormal basis of the Hilbert space L2(0,∞) . Closed-form expressions are derived for the matrix elements of H with re...

Insecticide application is the most common method of insect control in agriculture. Efficiency washing treatments reduction insecticide (chlorpyrifos-methyl and lambda-cyhalothrin) residues from grapes were investigated this study. The trial was established a Sultana seedless vineyard Sar?göl District, Manisa Province, Turkey 2020. Method verification performed with recovery, limit quantificati...

A capillary electrophoresis method was used for assay of some degradation products of carvedilol. The optimized parameters were as; running buffer 80 mM acetate dissolved in methanol/ethanol mixture (65:35 v/v), applied voltage of 19 kV, temperature is 20 ºC and the wavelength range of 200-350 nm. The results indicate that the proposed CE method could effectively separate carvedilol from its de...

The adsorption and removal of congo red from an aqueous solution by iron oxide nanoparticles (IONPs) coated with cetyltrimethylammonium bromide (CTAB) as adsorbent was reported. The novel magnetic separation was quite efficient for the adsorption and desorption of congo red. The effect of temperature, pH of aqueous medium, and interfering ions on the recovery process were also investigated. The...