نتایج جستجو برای: template removal
تعداد نتایج: 186024 فیلتر نتایج به سال:
coni nanowires were deposited by pulsed electrodeposition technique into porous alumina templates. the effect of off time between pulses (toff) and reductive/oxidative time (treduc/oxid) on the microstructure and magnetic properties of the coni nanowires were investigated. maximum coercivity and squareness were obtained for samples fabricated at treduc/oxid= 0.5 ms and toff =400 ms. the coerciv...
In this research, the zeolite sodalite, as an inorganic ion exchange material, was chemically produced in the template-free synthesis and evaluated in order to facilitate the sorption of strontium ions from aqueous solutions in batch operations onto acid treated zeolite with dilute H2SO4 solutions. The following indicates what the batch experiments included: a sorbent amount of 0.25 g in 100 mL...
organic solvents. In this study, NiFe2O4/sawdust nanocomposite was synthesized for removingoil pollutants. The oil-adsorbing nanocomposite could be easily separated from water bymagnet bar. The XRD results show tetragonal phase proving the composite formation. TheFESEM pictures successfully reveal the growth of NiFe2O4 on the sawdust template. The FTIRbands at 422 cm-1 and 615 cm-1correspond to...
In this study, simple ionic liquid-assisted preparation of SnO microflowers with nanosheet subunitsunder reflux condition without calcination were described. Samples were synthesized using 1-pentyl-3-methylimidazolium bromide, [pmim]Br, as an ionic liquid in different molar ratio, sodium hydroxideand Tin(II) chloride. The results show that SnO with high purity and uniform size...
Background: Electromyographic (EMG) signals obtained from a contracted muscle contain valuable information on its activity and health status. Much of this information lies in motor unit potentials (MUPs) of its motor units (MUs), collected during the muscle contraction. Hence, accurate estimation of a MUP template for each MU is crucial. Objective: To investigate the possibility of improv...
The aim of this work was synthesis of MCM-41/HA nanocomposite and biodegradation behavior of pure silica-mesoporous in attendance of hydroxyapatite crystals. These materials were synthsized by sol-gel method and ageing at 100°C for 24hr. A surfactant was used as template. The pores were formed after removal of surfactant by calcination at 550°C. FTIR results demonstrated formation of silanol a...
We report the preparation of [2]rotaxanes containing an electrochemically and optically active osmium(II) bipyridyl macrocyclic component mechanically bonded with cationic pyridinium axles. Such interlocked host systems are demonstrated to recognise and sense anionic guest species as shown by (1)H NMR, luminescence and electrochemical studies. The rotaxanes can be surface assembled on to gold e...
A ferrocene appended rotaxane is prepared by chloride anion templation and ring closing metathesis. Upon removal of the chloride template, the rotaxane is demonstrated to be selective for chloride over more basic oxoanions by (1)H NMR spectroscopy and electrochemistry, in marked contrast to an acyclic analogue--the first example of a solution based redox-active interlocked host system capable o...
the aim of this paper is eliminating cr(vi) by natural hap. hap is a inexpensive material which is used from bovine critical bone ash in order to remove heavy metal ions like cr(vi). some experiments in different ph are performed (ph=2,3,7). maximum adsorption was appeared at ph=2, dosage=0.3 gr, c0=10 mg/l. cr(vi) removal depends on ph value and initial amount of cr(vi) result of experiments w...
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