نتایج جستجو برای: x ray diffraction method
تعداد نتایج: 2226070 فیلتر نتایج به سال:
The use of plant extract is generating the interest of researchers toward cost effective,nontoxic, economic viability and eco-friendly green synthesis of nanoparticles. In the presentwork, zinc oxide (ZnO) nanoparticles were synthesized using black tea extract and zinc nitrateas the zinc source by the sol-gel method. The synthesized ZnO nanoparticles werecharacterized by powder X-ray diffractio...
Core-shell 12-tungstophosphoric acid/TiO2 (HPW/TiO2) nanoparticles at 10 and 20% of HPW have been synthesized by simple in-situ sol- gel method. Characterization of the samples was carried out by X-ray diffraction (XRD), Scanning electron microscopy (SEM), Fourier transform infrared (FTIR). The X-ray diffraction patterns of as prepared solid samples, indicated characterist...
where the peak shapes were described by a pseudo-Voigt function and the background was modeled with an 6-term polynomial. Additionally, the PXRD patterns obtained at room temperature and 100 K were analyzed by Le Bail refinement using the GSAS and EXPGUI software, 2,3 where the peak shapes were described by a pseudo-Voigt function (CW profile function 3) and the background was modeled with an 4...
Core-shell 12-tungstophosphoric acid/TiO2 (HPW/TiO2) nanoparticles at 10 and 20% of HPW have been synthesized by simple in-situ sol- gel method. Characterization of the samples was carried out by X-ray diffraction (XRD), Scanning electron microscopy (SEM), Fourier transform infrared (FTIR). The X-ray diffraction patterns of as prepared solid samples, indicated characterist...
Tellurium nanostructures have been prepared by physical vapor deposition method in a tube furnace. The experiments were carried out under argon gas flow at a pressure of 1 mbar. Tellurium powder was evaporated by heating at 350°C and 430°C and was condensed on substrates at 110–250°C, in the downstream of argon gas flow. The products were characterized by field emission scanning electron micros...
Tellurium nanostructures have been prepared by physical vapor deposition method in a tube furnace. The experiments were carried out under argon gas flow at a pressure of 1 mbar. Tellurium powder was evaporated by heating at 350°C and 430°C and was condensed on substrates at 110–250°C, in the downstream of argon gas flow. The products were characterized by field emission scanning electron micros...
In this paper, results from X-ray diffraction and the variation of electric resistance versus temperature of Gd3AuxAl1-x intermetallic compound are reported. All samples formed in orthorhombic crystalline structure with Pnma space group. In measuring the lattice parameters by X-ray diffraction method, deviation from Vegard’s rule has been seen. This deviation at x = 0.4 maximizes. In addition, ...
Oxide nanoparticles of Fe-Co-Ni were prepared in six different compositions by co-precipitation method. The as-synthesized nanoparticles were characterized by X-Ray Diffraction (XRD), Field Emission Scanning Electron microscope (FESEM), Fourier Transform Infrared (FT-IR) and Vibrating Sample Magnetometer (VSM). It was found that the nanoparticles had mean crystalline size of 30-55 nm and spher...
In the present work, we report a suitable approach for the preparation of BaTiO3 nanostructures via the hydrothermal condition using Dolapix ET85 as surfactant. The powders were investigated by X-ray diffraction (XRD), scanning election microscopy (SEM), energy-dispersive X-ray spectroscopy (EDAX), field emission transmission electron microscopy (FETEM), selected area electron diffra...
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