Synchrotron radiation based nanoscopic X-ray fluorescence (SR nano-XRF) analysis can visualize trace level elemental distribution in a fully quantitative manner within single cells. However, in-air XRF analysis requires chemical fixation modifying the cell's chemical composition. Here, we describe first nanoscopic XRF analysis upon cryogenically frozen (-150°C) fibroblasts at the ID16A-NI 'Nano...

century. The process involved polishing a silver coated copper plate, made photo sensitive by exposure to halogens, then exposed to light, and finally coated with gold. This complex, intricate process has yielded some of the most iconic images of the 19 th century. Unfortunately, in some instances plate interaction with storage materials have yielded objects ranging from pristine to disfigured....

Synchrotron-based micro-X-ray fluorescence (XRF) combined with scanning electron microscopy-based energy dispersive micro-analysis (EDS) has been used to determine the elemental distribution of contaminants (e.g., Ni) and of chemical elements inherent to the cement matrix (e.g., Si, Ca, Al, S) in hardened cement paste. Detailed information on the cement microstructure was gained by using backsc...

In vivo X-ray fluorescence (XRF) measurement of bone lead concentration (XRF) has emerged as an important technique for future epidemiological studies of long-term toxicity. Several issues germane to epidemiologic methodology need to be addressed, however. First, sources of variability in measurements of bone lead need to be quantified, including imprecision related to the physical measurement ...

Gold nanorods (GNRs) have been fabricated by a novel polymer-immobilised seed mediated method using ultraviolet (UV) photoreduced gold-polymethylmethacrylate (Au-PMMA) nanocomposites as a seed platform and characterised at sub-micron scale regime with synchrotron-based techniques; near-edge X-ray absorption fine structure (NEXAFS) spectroscopy and X-ray fluorescence (XRF) mapping. In this repor...

A test bench instrument constructed at MOXTEK, Inc. is capable of simultaneously capturing X-ray diffraction (XRD) and X-ray fluorescence (XRF) information using a charge-coupled device (CCD) as the X-ray detector. NASA is funding the instrument’s construction because of its low-power consumption and compact size; it could be used for in-situ planetary exploration missions for mineral analysis....

Non-destructive analysis of cultural objects by micro-XRF spectrometry is an advantageous multi-element technique that has rapidly developed during the past few years. Portable instruments contribute significantly to the in situ analysis of valuable cultural objects, which cannot be transported to the laboratory. Ancient ceramics are the most common archaeological findings and they carry a sign...

One of the advantages of X-ray fluorescence XRF analysis is its ability to perform accurate quantitative analysis over a wide range of elements with relative ease. In addition, its high sensitivity makes it ideal for trace elemental analysis. The establishment of analytical conditions for XRF is straightforward, including the determination of spectral line overlap correction factors. As with mo...