A novel, rapid, simple and sensitive dispersive liquid-liquid microextraction method based on the solidification of floating organic drop (DLLME-SFO) combined with high performance liquid chromatography-ultra violet detection (HPLC-UV) was used to determine acrylamide in potato chips. The derivation of the acrylamide happened in the presence of KBr, KBrO3, H2SO4. Based on studies, 1-undecanol w...

recently, subcritical water extraction (swe) has been well known as a green technology for extraction of bioactive compounds from plants. in this study, subcritical water extraction, ultrasound assisted extraction (uae) and shaker solvent extraction (sse) were compared for extraction of phenolic compounds from fig (ficuscarica) pulp and skin. antioxidant activity of the extracts was evaluated u...

Sea buckthorn oil (SBO) was extracted using accelerated solvent extraction with two green solvents (ethanol and 2-methyltetrahydrofuran), petroleum-based (hexane diethyl ether) at four different temperatures (60, 90, 120 150 °C), one cycle 103.42 bar, 10 min static time, 5 preheating 30% flushing volume. β-carotene α-tocopherol were quantified jointly HPLC-UV/VIS the fatty acid profile analyzed...

Isolation of carboxylic acids from dilute aqueous effluents can be achieved by the combination liquid-phase catalyzed reaction with liquid-liquid extraction. Exemplarily heterogeneously esterification acetic acid methanol, accelerated a cation-exchange resin and simultaneous transfer product methyl acetate into solvent ShellSol T, was successfully performed in Taylor-Couette disc contactor (TCD...

We have improved the method of measuring dioxins in the blood of Yusho patients; with this improved method, it is possible to take measurements quickly and precisely, using as little as 5g of blood. The specific points of improvement of this method are the extraction of lipids from blood by accelerated solvent extractor (ASE), the miniaturization of column cleanup for the purification of dioxin...

Residual N-methylcarbamate pesticides in food were determined by accelerated solvent extraction (ASE) and HPLC with post-column fluorescence. Pesticides were extracted with acetonitrile at 100 degrees C under 2000 psi pressure in less than 20 min. Extracts were cleaned-up with a carboxylic acid mini-column eluted with 10% or 30% acetone in hexane. Eight foods were spiked with 17 pesticides at 0...