Production of nickel-silver by mechanical alloying was investigated. Effects of parameters such as milling duration, ball to powder weight ratio, and chemical composition on mechanical alloying process, and alloys color and microstructure were studied. The milled powders were characterized, using XRD and SEM. Results showed that nickel-silvers could be produced by mechanical alloying in a wide ...

The solid state reactions and structural evolution in nanocrystalline FePt powders during mechanical ball milling at 77 K and subsequent annealing have been investigated. Above 310 °C the formation of L10 FePt is observed. As the milling time increases, the enthalpy evolved during the transformations is reduced, whereas the corresponding activation energy increases. For accelerating the orderin...

Tailor-made additives can prove an effective method to prolong the lifetime of metastable forms of pharmaceutical compounds by surface stabilization. Pyrazinamide (PZA) is a pharmaceutical compound with four polymorphic forms. The high temperature γ form, which can be produced by spray drying or sublimation growth, is metastable at room temperature and transforms within days when produced by sp...

Due to its relatively low cost, high hydrogen yield, and environmentally friendly hydrolysis byproducts, magnesium hydride (MgH2) appears to be an attractive candidate for hydrogen generation. However, the hydrolysis reaction of MgH2 is rapidly inhibited by the formation of a magnesium hydroxide passivation layer. To improve the hydrolysis properties of MgH2-based hydrides we investigated three...

Hydrolysis is an efficient way of producing hydrogen by using Mg-based waste. In this study, H2 production realized in simulated seawater (i.e., 3.5 wt.% NaCl) the Elektron21 (EL21) alloy as a reagent. This magnesium-based composed 96 Mg and 4 rare earth (approx. 3 Nd 1 Gd). EL21 known for its excellent corrosion resistance high tensile strength. The impact different mechanical treatments (ball...

The mechanochemical dechlorination of pentachlorophenol (PCP) was studied using CaO and SiO2 powder as additives. The effects of the milling time and additives on the dechlorination rate were investigated. The resulting product was characterized by X-ray diffraction (XRD), Fourier transform infrared spectra (FT-IR), thermogravimetric analysis (TG) and ion chromatography (IC). It is found that g...

The compound Mg 2 FeH 6 was synthesized from a 2Mg-Fe mixture in a single process through high-energy ball milling under hydrogen atmosphere at room temperature. The complex hydride was prepared from Mg powder and granulated or powdered Fe using a planetary mill. The phase evolution during different milling times was performed by X-rays diffraction technique. The dehydrogenation behavior of the...

The mechanism of milling-induced amorphization was studied by investigating the structural evolution during amorphization via high-energy ball milling of a chalcogenide compound, i.e. Ag3PS4 crystal. The gradual decrease in intensity of the XRD diffraction peaks of Ag3PS4 milled for different durations indicates that the degree of amorphization was enhanced by the mechanical milling. The forwar...

The aim of this study was to develop optimized sucrose ester (SE) stabilized oleanolic acid (OA) nanosuspensions (NS) for enhanced delivery via wet ball milling by design of experiments (DOE). In this study, SEOA NS batches were prepared by wet ball milling method. Mean particle sizes and polydispersity indices were determined using a nanosizer. The percent encapsulation efficiency, saturation ...

The process of ball milling and the materials that compose planetary mills are highly complex, existing research on change in ball-milling energy is not mature. theoretical model a mill was established for first time to simulate motion, collision process, transfer, temperature small balls during process. Furthermore, by comparing information with experimental data mill, motion trajectory grindi...