Materials that are functionally graded and have a layered structure made of nickel aluminum were fabricated by powder metallurgy procedure. Al/Ni FGM consist five layers. The material sample starts with pure ends nickel. the layers (25 Ni-75Al) %, (50 Ni-50 Al) % (75 Ni-25Al) %. Samples sintered at temperature 600° C. Apparent density, green porosity, shrinkage each layer measured.