High energy 2D X-ray powder diffraction experiments are widely used for lattice strain measurement. The 2D to 1D conversion of diffraction patterns is a necessary step used to prepare the data for full pattern refinement, but is inefficient when only peak centre position information is required for lattice strain evaluation. The multi-step conversion process is likely to lead to increased error...

Nanocrystalline Zinc Oxide (ZnO) powders with different morphology have been successfully synthesized by using different surfactants such as Cetyl Trimethyl Ammonium Bromide (CTAB), Sodium Dodecyl Sulphate (SDS), and Tri Ethanol Amine (TEA) via hydrothermal method. The products were characterized by means of powder X-ray diffraction (XRD), Scanning electron microscopy (SEM), Transmission electr...

tio2 nanorods can be used as dye-sensitized solar cells and as various sensors and photocatalysts. these nanorods are synthesized by a using thermal corrosion process in a naoh solution at 200 oc with tio2 powder as a source material. in the present work, the synthesis of tio2 nanorods in anatase, rutile and ti8o15 phases and the synthesis of tio2 nanorods by using the sol-gel method and alkali...

Hydroxyapatite nanorods aligned with ultrahigh crystallinity and high-yield were successfully synthesized through a hydrothermal approach. In this experiment, a new composition of cetyltrimethylammonium bromide ((CH3(CH2)15N+(CH3)3Br-) was designated as CTAP)/Ca(NO3)2/(NH4)2HPO4/NaOH and distilled water under hydrothermal condition, to synthesize single crystalHAp nanorods with diameter of 20 ±...

This paper introducesminiPixD: a new, compact system that utilises transmission X-ray imaging and X-ray diffraction (XRD) to locate and identify materials of interest within an otherwise opaque volume. The system and the embodied techniques have utility in security screening, medical diagnostics, non-destructive testing (NDT) and quality assurance (QA). This paper outlines the design of the sys...

A novel method which is based on the hydrothermal reaction was employed to synthesize LiV3O8. First, the mixture solution of LiOH, V2O5, and NH4OH was subjected to the hydrothermal reaction. The hydrothermal treatment yielded a clear, homogeneous solution. The evaporation of this solution led to the formation of a precursor gel. The gel was then heated at different temperatures in the range of ...

     In a hydrothermal route devoted for synthesis of Ca10(PO4)6(OH)2 (HA) nanostructures, morphology can be controlled by experimental condition to form magical HA or nanostructured nanoparticles. In an intermediate condition, a novel nanostructure namely rose-like bundle of HA rod-likes was found, which is different from known HA nanostructures. The...

this paper presents a systematic study of the surface chemistry, porous texture and adsorptive characteristics of prepared new activated carbon using persian mesquite grain. several techniques and methodologies such as, proximate analysis, n2 adsorption–desorption isotherms, scanning electron microscope (sem), fourier transform infrared spectroscopy(ft-ir), x-ray diffraction (xrd), x-ray photoe...

Copper nanoparticles/fluorine-doped tin oxide (FTO) nanocomposites were successfully prepared by a simple hydrothermal method. The synthesized nanocomposites were characterized by X-ray diffraction (XRD), UV-visible diffuse-reflectance spectrum (UV-VIS DRS), energy dispersive X-ray (EDX), transmission electron microscopy (TEM), Raman spectra, and X-ray photoelectron spectroscopy (XPS). The obta...

In this study, pyrite was produced by hydrothermal precipitation from the reaction between FeSO4 and Na2S2O3 at high pressure and high temperature in a stirred reactor. The solid product was purified by means of solvent extraction to remove sulfur. Powder was characterized by X-Ray Diffraction (XRD), Scanning Electron Microscopy (SEM) and thermal ...