نتایج جستجو برای: pot synthesis

تعداد نتایج: 417578  

Bahareh Sadeghi, Fereshteh Karimi

1,2-Diketones have been reacted in one-pot method with 1,2-diamines at room temperature with ZnO nanoparticles as a catalyst. ZnO nanoparticles as an available and reusable catalyst is used for the synthesis of Quinoxalinein improved yields.

Fatemeh Kooti Gholam Hossein Mahdavinia, Hamid Sepehrian Mohammad Mehdi Ghanbari

MCM-41-R-SO3H catalyzed one-pot synthesis of 1,8-dioxo-octahydroxanthenes is reportedunder reflux conditions. The catalyst is easily prepared, highly stable, very simple to handle andrecycled for five times without loss of significant activity

Journal: :organic chemistry research 2015
saeed balalaie fatemeh tahoori negin khatibi

a simple and efficient one-pot, three-component strecker reaction of protected amino acids, aromatic aldehydes, and trimethylsilyl cyanide has been developed for the synthesis of chiral α-amino nitriles. the reaction was carried out in the presence of catalytic amount of phosphotungstic acid (h3[p(w3o10)4]) as an environmentally friendly catalyst.

Journal: :journal of nanostructures 2012
j. safaei-ghomi m. a. ghasemzadeh

the efficient and environmentally friendly method for the one-pot synthesis of polyhydroquinolines has been developed in the presence of cuo nanoparticles. the multi-component reactions of aldehydes, dimedone, ethyl acetoacetate andammonium acetate were carried out under solvent-free conditions to afford some polyhydroquinoline derivatives. this method provides several advantages including high...

Journal: :iranian journal of catalysis 2012
farhad shirini gholam hossein imanzadeh masoumeh abedini maryam akberi dokhte-ghaziani mohaddeshes safarpoor langroodi

1,3-dibromo-5,5-dimethylhydantoin (dbh) and benzyltriphenylphosphoniumtribromide (btptb) were used as efficient catalysts for the promotion of the synthesis of 1,8-dioxo-octahydroxanthene derivatives (doxos) via a one-pot three component condensation of aldehydes and cyclic 1,3-dicarbonyl compounds in the absence of solvent.

Journal: :iranian journal of catalysis 2014
hossein naeimi zahra sadat nazifi

efficient and one-pot synthesis of 1,8-dioxo-octahydroxanthenes was described by knoevenagel condensation, michael addition and cyclodehydration of dimedone. this reaction was carried out through condensation of dimedone and various aromatic aldehydes in the presence of task-specific brønsted acidic ionic liquid under solvent free conditions. the catalyst could be recycled five times without si...

Journal: :organic chemistry research 2015
khodabakhsh niknam nassim - borazjani

silica-bonded n-propyldiethylenetriamine sulfamic acid (spdtsa) is employed as a recyclable heterogeneous solid acid catalyst for the synthesis of benzopyrano[2,3-d]pyrimidines  through one-pot condensation reaction of salicylaldehydes, malononitrile and secondary amines  at room temperature under solvent-free conditions. spdtsa showed much the same efficiency when used in consecutive reaction ...

The one-pot synthesis of symmetrical triaryl amines using aryl halides and 5-Methyl-1,3,4-Thiadiazole-2-Amine as a nitrogen-transfer reagent is reported. Copper oxide nanoparticles that does not require the presence of any additional ligand, improved rate and facility of the synthesis of triaryl amines. The introduction of a new N-source, using green solvents PEG/H2O, normal atmospheric conditi...

Journal: :iranian journal of chemistry and chemical engineering (ijcce) 2004
ali kakanejadifard s. morteza farnia golamreza najafi

the one pot reaction of glyoxal and hydroxylamine hydrochloride in aqueous sodium hydroxide was found to be a safe and inexpensive method for the preparation of diaminoglyoxime. by increasing stoichiometric ratio of the hydroxylamine hydrochloride and decreasing the solvent volume, the product yield increased considerably (~ 70%).

Journal: :iranian journal of catalysis 2015
khatereh khandan-barani arezo motamedi-asl

for the first time lactic acid was applied as an efficient and green catalyst for the one-pot three-component synthesis of amidoalkyl naphthols via the condensation between arylaldehydes, 2-naphthol and amides or urea under thermal solvent-free conditions in good to excellent yields. we have demonestrated a mild and efficient eco-friendly tandem synthesis of amidoalkyl naphthols using lactic ac...

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