a new nano-sized cobalt(ii) coordination polymer, (col1).0.5dmf.1.5ch3oh(1); [h2l1 = 5-(4-carboxy phenyl azo) salicyilic acid] has been synthesized by a sonochemical method. the thermal stability of compound 1 was studied by thermo- gravimetric and differential thermal analyses. nano-structure of this coordination polymer was characterized by elemental analyses, ir spectroscopy,  powder x-ray d...

The value of t he scanning e lec t ron microscopy i n p rov id ing i n s i t u i n fo rma t ion on t h e microst ructure o f ma te r ia l s such as coal I s we l l known. m a r t i c u l a r l y su i ted for examining the f i n e l y d i s t r i b u t e d mineral p a r t i c l e s found i n f ine ly-ground coal. data can be provided. c a l analysis t o be performed on these minute features, thu...

The strain of P. aeruginosa used was a Fisher serotype 3,7, originally isolated from a patient with severe burns. The susceptibility of the strain to antibiotics used singly and in combination was determined by the tube dilution method (12). Minimal inhibitory concentrations (MICs) were determined by observing the lowest dilution of antibiotic that prevented visible growth of an inoculum of 105...

introduction: presence of surface defects in endodontic instruments can lead to unwanted complications such as instrument fracture and incomplete preparation of the canal. the current study was conducted to evaluate the effect of autoclave cycles on surface characteristics of s-file by scanning electron microscopy (sem). methods and materials: in this experimental study, 17 brand new s-files (#...

in this work, the effects of acetic and lactic acids addition to rice during cooking, on the texture and morphological properties, and too, the gelatinization temperature (gt) of the cooked domsiyah rice was investigated. all experiments were carried out in triplicate and data analyzed in randomized completely by spss15 software. the results showed that acid addition to rice during cooking caus...

introduction radiotherapy planning systems require many percentage depth dose (pdd) and profile measurements and there are various dosimeters that can be used to obtain these scans. as dose perturbation is particularly troublesome in smaller photon fields, using a low-perturbation, unshielded electron field diode (efd) in these fields is of interest. the aim of this work was to investigate the ...

sol–gel auto-combustion is a unique combination of the combustion and the chemical gelation processes. in this work, nanosize (d) powders with compositions of znfe2o4 were synthesized by sol–gel combustion method. the puffy, porous brown powders as-combusted was calcined at the temperature of 750–1000◦c for 4 h. these powders are characterized by x-ray diffraction and scanning electron microsco...

cadmium oxide (cdo) nanoparticles were prepared by precipitation method using cadmium acetate and ammonia solution. presence of chemical species, were verified by fourier transform infra red (ftir) spectrum. from x-ray diffraction (xrd) spectrum the particle size, d-spacing value and structure of the nanoparticle were analysed. size of the nanoparticles and the elemental composition were detect...

friction stir processing was applied for fabricating an aluminum alloy based hybrid nano composite reinforced with nano sized al2o3 and micro sized graphite particles. a mixture of al2o3 and graphite particles was packed into a groove with 1 mm width and 4.5 mm depth, which had been cut in 5083 aluminum plate of 10 mm thick. packed groove was subjected to friction stir processing in order to im...

the characterizations of natural diatomite from birjand deposit (iran) were studied such as chemical compositions, specific surface area, total pore volume, pore size distribution and xrd. the diatomite that was treated only with sulfuric acid displayed a larger surface area, expanded total pore volume and increased pore size in comparison with both washed natural diatomite with deionized water...