نتایج جستجو برای: sem edx
تعداد نتایج: 66382 فیلتر نتایج به سال:
The paper aims on the investigations of corrosion processes of three different porcelain fused to metal dental crowns with CoCrMo frameworks. The three crowns, with different exposed metal surfaces, were investigated using electrochemical impedance spectroscopy (EIS), through 168 hours of experiment. The data were analyzed and the influence of corrosion processes was shown after the crowns were...
Gold Mosaic glass has been used to decorate items and places since ancient time. The glass structure is divided into three layers: cover glass, gold layer and glass substrate. In this study, the composition of old-styled Thai gold mosaic glass samples was analyzed using SEM/EDX and Raman spectroscopy. It was found that the glass composition was sodiumsilicate based glass. Raman spectroscopy als...
Thermodynamic analysis and characterization of the investigated Ga-Ge-Sb alloys, which is of a practical importance in electric semiconductors industry, are presented in this paper. Thermodynamic analysis are done by the used of experimental investigation technique of Oelsen calorimetry and different thermal analysis (DTA) and thermodynamic predicting methods, while characterizations are done b...
The data presented in this article are related to the research article entitled: "Solder free joining as a highly effective method for making contact between thermoelectric materials and metallic electrodes" (Malik et al., 2017) [1]. This article presents microstructure obtained by scanning electron microscopy (SEM) and chemical analysis by energy dispersive X-ray spectroscopy (EDX) point measu...
Amorphous Spherical Carbon with Nitrogen (SCN) active carbon has been prepared by carbonization of poly(vinylpyridine-divinylbenzene) (PVPDVB) copolymer. The PVPDVB dehydrogenation copolymer has been quantum chemically (QC) simulated using cluster and periodic models. Scanning electron microscopy (SEM), transmission electron microscopy (TEM) and energy dispersive X-ray (EDX) studies of the resu...
In this work, the influence of the substrate bias on the crystalline structure and surface composition of Ti6Al4V thin films prepared by rf magnetron sputtering were studied. Samples were grown onto two different types of substrates: AISI 420 steel and common glass using a Ti6Al4V (99.9 %) target. Substrate bias was varied from –100V to –200 V. Samples were characterized by X-ray diffraction (X...
Aim: To assess the surface topography and chemical composition of three brands of as-received mini-implants (SIN®, Morelli®, and Conexao®). Methods: Twelve mini-implants of each brand were analyzed by scanning electron microscopy and energy dispersive X-ray (EDX). Results: There was no significant differences among SIN®, Morelli®, and Conexao® mini-implants comparing their surface topography by...
In this work ZnO and Mn-doped ZnO nanocrystals were synthesized by one-step aqueous solution method. X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive x-ray (EDX) analysis and photoluminescence (PL) spectroscopy have been used to characterize the samples in detail. The XRD studies revealed that the ZnO and Mn-doped ZnO had wurtzite structure (hexagonal). The composi...
The mineral yuksporite (K,Ba)NaCa2(Si,Ti)4O11(F,OH)⋅H2O has been studied using the combination of SEM with EDX and vibrational spectroscopic techniques of Raman and infrared spectroscopy. Scanning electron microscopy shows a single pure phase with cleavage fragment up to 1.0 mm. Chemical analysis gave Si, Al, K, Na and Ti as the as major elements with small amounts of Mn, Ca, Fe and REE. Raman ...
In the frame of the European project NanoValid, potential candidates of reference nanomaterials are manufactured and systematically characterized in particular with respect to their morphology (shape, size and size distribution). In this study, by exploiting the transmission operation mode in a high-resolution SEM, known as transmission SEM, the potential of this methodical approach is demonstr...
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