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a novel podand based anion receptor bearing benzimidazole motifs as recognition sites was designed and synthesized by reaction of 1,7-bis(2'-methylbenzoate)-1,4,7-trioxaheptane and phenylenediamine. the binding properties of anionic guest with this receptor were studied using uv-vis and fluorescence spectroscopy. these studies revealed that this receptor exhibit selective recognition towards f- ...

the main objective of this research was to synthesize and characterize gold-coated fe3o4 /sio2 nanoshells for clinical applications. magnetite nanoparticles (nps) were prepared via co-precipitation. the results showed that smaller particles can be synthesized by decreasing the naoh concentration, which in our case this corresponded to 35 nm by using 0.9 m of naoh at 750 rpm. the nps were then m...

polymer-clay nanocomposite coatings have attracted much attention because of impressive enhancements of coating properties. in this research, both commercially available and isophoronediamine-modified montmorillonite clays were used to obtain epoxy-clay nanocomposite coatings. these nanocomposite materials with different clay loadings in the form of coatings were applied to cold-rolled steel (c...

schiff base sal-2,5-clan = 2-(2,5-dichlorobenzylideneamino)phenol used as a new precursor for preparation of poly-2-(2,5-dichlorobenzylideneamino)phenol (pdcbap). in an aqueous alkaline medium, naocl oxidant is capable of oxidative poly-condensation reaction (op). both sal-2,5-clan and pdcbap were characterized by solubility tests, ft-ir, 1h-nmr spectroscopy and tg-dta studies. ft-ir and 1h-nmr...

a r t i c l e i n f o a b s t r a c t In the context of sample evidence alone, the high-alumina (HA) basalts appear to be an unique, and rare variety of mare basalt. In addition to their distinct chemistry, radiometric dating reveals these basalts to be among the oldest sampled mare basalts. Yet, HA basalts were sampled by four missions spanning a lateral range of ∼2400 km, with ages demonstrat...

aim: to enhance the aqueous solubility of olanzapine by using the solid dispersion technique. solid dispersions of olanzapine were prepared by the dispersion method using using pgs and ssg as carriers. drug:carrier ratios such as 1:1, 1:2, 1:4, 1:6, 1:8 and 1:10 were tried for optimization. characterization was done by phase solubility, in vitro release, saturation solubility, permeation, wetta...

background: distinction between radiation necrosis and recurrence of intraparenchymal tumors is necessary to select the appropriate treatment, but it is often difficult based on imaging features alone. we developed an algorithm for analyzing magnetic resonance spectroscopy (mrs) findings and studied its accuracy in differentiation between radiation necrosis and tumor recurrence. m e t hod s :  ...

bioactive materials including glass and glass-ceramics are nowadays used as medical implants for orthopedic applications. in this study several samples of glass-ceramics have been prepared using both heat treatment and sol-gel processes. the structure and bioactivity of these samples based on their interaction with simulated body fluid (sbf) have been determined. in-vitor, using the raman spect...