lead forms the complexes with xylenol orange in the basic solution. an adsorptivedifferential pulse stripping method for the determination of lead is proposed. the procedureinvolves an adsorptive accumulation of lead on a hanging mercury drop electrode (hmde) inthe presence of xylenol orange, followed by reduction of adsorbed lead by voltammetric scanusing differential pulse modulation. the opt...

This work describes a new type of integrated lab-on-a-membrane foldable device suitable for on-site duplex electrochemical biosensing using drop-size sample volumes. The devices are fabricated entirely by screen-printing on a nylon membrane and feature two assay zones which are located symmetrically on either side of a three-electrode voltammetric cell with a bismuth citrate-loaded graphite wor...

the voltammetric behaviour of sulfadoxine (sdn) was studied at a glassy carbon electrode in 0.2 m phosphate buffer solutions using cyclic, differential-pulse (dpv) and square wave voltammetry (swv). the dependence of the current on ph, concentration, and scan rate was investigated to optimize the experimental conditions for the determination of sdn. the oxidation process was shown to be diffusi...

Development of sensitive and selective methods to detect proteins at trace levels is of great biological importance. Via derivatization with a bifunctional cross-linker 4-maleimidobutyric acid N-hydroxysuccinimide ester (GMBS) and an electrochemical marker 11-ferrocenyl-1-undecanethiol (Fc-SH), voltammetric determination of surface-confined proteins electrostatically adsorbed onto the polyelect...

Voltammetric detection of metals in natural waters suffers from interference by dissolved oxygen. We describe here a deoxygenation method suitable for ̄ow analysis with detection by cathodic stripping voltammetry (FIA-CSV). The apparatus is based on the permeation of oxygen through semi-permeable tubing (silicone, Pore ̄on and others) into an oxygen-free chamber. Two methods of oxygen removal ar...

This paper presents an accurate and fast electrochemical method for atorvastatin determination in pharmaceutical products. Two screen-printed sensors, one—carbon based (SPCE) one on carbon nanotubes gold nanoparticles (AuNP-CNT/SPCE) were used during the analyses. At all experimental stages, cyclic voltammetry was employed, both characterization of sensors their behavior, quantitative determina...