-The chemical composition of mixed-layer serpentine/chlorite (Sp/Ch) in Tuscaloosa Formation sandstone was analyzed by energy dispersive X-ray spectroscopy (EDX) in the scanning electron miscroscope (SEM) and by X-ray diffraction (XRD). EDX results indicate little depth-controlled variation in composition, whereas XRD results suggest distinct decreases in octahedral Fe and tetrahedral A1. XRDde...

the magnetite (fe3o4) – agar nanocomposite was prepared by co-precipitation of fe (iii) and fe (ii) ions for the first time. the obtained samples were characterized by x-ray diffraction, fourier-transform infrared spectroscopy, scanning electron microscopy and transmission electron microscopy. ft-ir results confirm the formation of fe3o4 nanoparticles in agar matrix. the xrd results revealed th...

co-fe films were electrodeposited on cu substrate from electrolytes with different co concentration  levels. x-ray diffraction (xrd) was used  to  investigate  the  films  crystal  structures. the  results  indicate that  if  the  co  concentration  is  less  that  the  fe  concentration,  the cubic  structure  appears  in  the  films, while  the  hexagonal  structure dominates when  the co  co...

Layered double hydroxides (LDHs) exhibit characteristic anion-exchange chemistry making them ideal carriers of negatively charged molecules like deoxyribonucleic acid (DNA). In this study, hydrotalcite (Mg-Al) and hydrotalcite-like compounds (Mg-Fe, Zn-Al, and Zn-Fe), also known as LDHs, were evaluated for their potential application as a carrier of DNA. LDHs were prepared by coprecipitation at...

The effect of small amounts of ruthenium on the formation of magnetite in highly alkaline media was investigated using X-ray powder diffraction (XRD), Mössbauer and FT-IR spectroscopies, field emission scanning electron microscopy (FE-SEM) and energy dispersive X-ray spectroscopy (EDS). Acicular a-FeOOH particles precipitated in a highly alkaline medium with the addition of tetramethylammonium ...

i ii iii iv Dedicated to my mother… v ACKNOWLEDGEMENTS This thesis would simply not have been possible without the work, guidance and endless belief and support of my guide Dr. S. Vijayalakshmi. She really did show me what it takes to pursue research and kept me going. Her patient, modest and kind nature helped me understand and do better. Her warm words of appreciation and encouragement made m...

The microbiologic reduction of a 0.2 to 2.0 mm size fraction of an Atlantic coastal plain sediment (Eatontown) was investigated using a dissimilatory Fe(III)-reducing bacterium (Shewanella putrefaciens, strain CN32) to evaluate mineralogic controls on the rate and extent of Fe(III) reduction and the resulting distribution of biogenic Fe(II). Mössbauer spectroscopy and X-ray diffraction (XRD) we...

The effect of different calcination temperatures on molecular structure, morphology, and antioxidant activity was investigated for Zinc Oxide nanoparticles synthesized using the sol-gel method capping agent Spirulina platensis. prepared nanoparticle ZnO calcined at 160°C, 300°C, 600°C according to results DTA-TGA analysis. characterization samples studied Fourier Transform Infrared (FTIR), X-ra...