In order to investigate certain aspects of protein metabolism, it was desired to prepare glycine labeled with radioactive carbon. The method of preparation was chosen with the object of obtaining the highest possible yields, and techniques suitable for handling small amounts of material were used throughout. The reactions employed and the yields obtained were as follows: The synthesis involves ...

We developed an analytical reverse-phase high-performance liquid chromatographic procedure for rapid assessment of the purity of NADH. The method completely separates adenosine monophosphate and adenosine diphosphoribose from NADH. By use of this analytical technique we found that preparative chromatography on DEAE-cellulose gives NADH that is free from adenine nucleotides as well as other impu...

The conversion of steelmaking slag (a waste product of the steelmaking process) to calcium carbonate (CaCO(3)) was tested using hydrochloric acid, ammonium hydroxide and carbon dioxide via a pH-swing process. Batch reactors were used to assess the technical feasibility of calcium carbonate recovery and its use for pre-treatment of acid mine drainage (AMD) from coal mines. The effects of key pro...

The potential of Helicobacter pylori to degrade gastric mucus was examined. Colonies of H pylori cultured from antral mucosal biopsy specimens of patients with non-autoimmune gastritis were washed with sterile saline, passed through a sterilisation filter, and the filtrate examined for urease, protease, and mucolytic activity. The filtrate failed to hydrolyse bovine serum albumin, or to degrade...

In the deltaic plain of the Ganges-Meghna-Brahmaputra rivers, arsenic concentrations in groundwater commonly exceed regulatory limits (50 μg l) because FeOOH is microbially reduced and releases its sorbed load of arsenic to groundwater. Neither pyrite oxidation nor competitive exchange with fertilizer-phosphate contribute to arsenic pollution. The most intense reduction, and so severest polluti...

This paper reports on the development and verification of a new simple, rapid and accurate titration method suitable for on-site measurement of volatile fatty acids (VFA) and carbonate alkalinity in anaerobic reactors. The method takes into account the effects of the phosphate, ammonium, sulfate, and sulfide weak acid subsystems on titration results. The method involves eight pH observations an...

The parameters to prepare U3O8 by calcination from ammonium uranyl carbonate were optimized by using response surface methodology. A quadratic equation model for the value of total uranium and U4+ of triuranium octaoxide was built and the effects of main factors and their corresponding relationships were obtained. The statistical analysis of the results indi...

Treatment of apatite raw materials is associated with the formation large-tonnage waste – phosphogypsum. The content rare earth metals in such reaches 1 %, which makes it possible to consider a technogenic source for obtaining and their compounds. Up present moment, there are neither processing plants, nor an efficient process flow handle phosphogypsum dumps. It rational use way that involves e...