In this paper, we report the comparison between TiO2 nanoparticles prepared via two different routes; i) via sol-gel route and ii) by hydrothermal method. It was found that when prepared under the same ambient conditions viz temperature, pressure etc. and keeping all the parameters same viz precursors, mole ratio, solvent etc; the nanoparticles prepared via sol-gel route were highly crystalline...

X-ray powder diffraction of red kangaroo (Macropus rufus) dental enamel, with a relative density greater than 2.60, showed a longer a-axis length of the apatite unit cell, a = 9.462 A, a shorter c-axis length, c = 6.877 A, and a smaller crystallite size, ca. 185 A, than those of human dental enamel. The a-axis of red kangaroo dental enamel was one of the longest among the values reported previo...

We explore the effects of crystallite size (L(a)) on the linear and non-linear optical properties of chemical vapor deposition grown polycrystalline graphene. The π-plasmon resonance present at ∼4.75 eV (∼260 nm) in the optical absorption spectrum of graphene follows the empirical relationship λ(π) = 250.5 nm + 89.5 nm(2)/L(a), where λ(π) represents the π-plasmon wavelength. Furthermore, our Z-...

In a hydrothermal preparation of crystalline magnetite (Fe3O4) nanoparticles, the influence of the experimental parameters (initial molar ratio of ferrous/ferric ions, initial concentration of ferrous ions, and heating time), and their interactions, on the particle formation was studied using response surface methodology (RSM), based on a statistical design of experiments (DOE). As indices indi...

Superparamagnetic single phase zinc ferrite nanoparticles have been prepared by coprecipitation method at 20 °C without any subsequent calcination. The composition, crystallite size, microstructure and magnetic properties of the prepared nanoparticles were investigated using X-ray diffraction (XRD), field emission scanning electron microscope (FESEM), transmission electron microscope (TEM)...

In this work, Ce0.75Gd0.1Ca0.15O1.8 nanopowders are successfully synthesized by a Glycine-nitrate combustionprocess under the microwave irradiation. Then calcination was carried out at 700 °C. Calcined powdersidentified by room temperature X-ray diffraction were single phase and had a crystallite size between 16 to 24nm (based on Schererr formula). Scanning electron microscopy (SEM) was employe...

this study reports the simple process to synthesis of cuo/cui nanocomposite in a non-aqueous solution. in the conducted experiments cui and dimethyl sulfoxide (dmso) were used as the precursors. moreover, dmso had role of solvent and ligand simultaneously. in experiments the effects of oleic acid as the particles size modifier, temperature and concentration were investigated. crystalline struct...

cd1-xmnxs (x = 0, 0.1, 0.2) nanoparticles, prepared by co-precipitation method under ultrasonic irradiation, were studied by means of x-ray diffraction, scanning electron microscopy, ftir and uv-vis  spectroscopy measurements. the average particle size of nanoparticles from the scanning electron microscopy image is about 20-30 nm. results show that partial substitution of cd by mn leads to a re...