A very simple, rapid and sensitive dispersive liquid-liquid microextraction (DLLME) followed by gas chromatography and flame ionization detection (GC-FID) was developed for the determination of phenol and carvacrol in honey samples. A mixture of 100 μl dichloromethane (extraction solvent) and 0.5 ml acetonitrile (disperser solvent) was rapidly injected into sample solution. Thereby a cloudy sol...

Detection and separation of metals from fresh water and industrial effluents has become a pre-requisite for any nation in the world. In and around the city of Hyderabad (Sindh), Pakistan, the home as well as cottage industry which consumes chemicals containing the copper, mercury, cadmium and lead are freely dumped into local ravines and canals unchecked for many years. The process is polluting...

an air–assisted liquid–liquid microextraction method for the extraction and preconcentration of trace amounts of some synthetic phenolic antioxidants in biological fluids followed by their determination by gas chromatography–flame ionization detection has been reported. in this method the target analytes are extracted into a few microliters of carbon tetrachloride (extraction solvent) from an a...

1. Survey 1.1. Characteristics to be analyzed 1.2. Concentration Units 1.3. Presentation of Analytical Results 1.4. Quality of Analyses 1.5. Analytical Procedures 2. Flue Gas Sampling 2.1. Sampling Effluents 2.2. Organic Micropollutants Sampling 2.3. Gas Sampling Train 2.4. Sampling of Inorganic Compounds 3. Gas Analyzers 3.1. Survey 3.2. Gas Chromatographic Separation 3.3. Gas Chromatographic ...