In this study, the Zn/Al-TiO2 and Zn/Al-ZnO was successfully synthesized. The catalysts were characterized by X-ray Diffraction (XRD), Fourier Transform Infra Red (FTIR), Scanning Electron Microscope—Energy Dispersive Spectroscopy (SEM-EDS). typical diffraction peaks of Zn/Al-LDH, TiO2, ZnO still appear in composites, indicating that composite preparation did not change form precursors. FTIR sp...