نتایج جستجو برای: process parameters sol gel methods
تعداد نتایج: 3427084 فیلتر نتایج به سال:
Two-typed (3-mercaptopropyl)trimethoxysilane-based networks which had been used to fabricate biosensors were prepared on Au substrates by two methods: layer-by-layer assembly, and the combination of sol-gel and self-assembly process. The formation mechanism and their surface properties, as well as stabilities were examined by cyclic voltammetry, electrochemical impedance spectroscopy, and X-ray...
The high quality properties and benefits of graphene-oxide have generated an active area of research where many investigations have shown potential applications in various technological fields. This paper proposes a methodology for enhancing the pyro-electricity of PVDF by graphene-oxide doping. The PVDF film with graphene-oxide is prepared by the sol-gel method. Firstly, PVDF and graphene-oxid...
Sol-gel derived silica possess many promising features, including low-temperature preparation procedure, porosity, chemical and physical stability. Applications exploiting porous materials to encapsulate sensor molecules, enzymes and many other compounds, are developing rapidly. In this paper some potential applications, with emphasis on biomedical and environmental ones, are reviewed. The mate...
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Thin films of ZnO grown by sol-gel spin method using two different precursors viz. zinc nitrate and zinc acetate have been characterized for their crystalline nature and associated nanostructures. In some cases, the films consist of nanostructures in the form of nanocrystals and nanoneedles of dimensions in the range 15-60 nm. A comparison between the physical characterization and the nanostruc...
In this communication we present a new sol–gel route to obtain high quality BaFe12O19 thin films. X-ray analysis confirmed the crystal structure with a crystal size of 32 nm. Atomic force microscopy images determined the film thickness to be around 250 nm and a roughness factor of less than 40 nm where the grain size averaged around 150 nm. SQUID magnetometer data shows a magnetic behavior simi...
Homogeneous thick silica coatings were prepared onto metals substrates by Electrophoretic Deposition (EPD) using particulate sol-gel sols. The synthesis of the sols was performed by mixing tetraethoxysilane and methyltriethoxysilane under basic catalysis. The synthesis, storage and processing conditions were optimised, correlating the rheological properties of the sols with EPD performance and ...
In the Present work structural, morphological and compositional properties of ZnO nanopowders synthesized using Zinc nitrate and NaOH using sol-gel process were reported. The synthesized nanopowders were further analyzed using X-Ray Diffraction (XRD), Scanning electron microscopy (SEM) and Fourier Transform Infrared (FTIR) spectroscopic characterizations. Crystalline size and Lattice strain det...
In this paper, we report the synthesis, the characterization and the scintillation properties of sol-gel derived Lu 2 SiO 5 (LSO) powders. Ce 3+ , Eu 3+ and Tb 3+ doped LSO powders have been synthesized by an original sol-gel process. The purity of the materials has been checked by X-Ray diffraction, confirming the elaboration of monophasic powders even for doped samples. Finally, the scintilla...
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