This application note describes a sensitive and reliable method for the determination of perfluorinated carboxylic acids (PFCAs) in human plasma. PFCAs were extracted from a plasma sample using an optimized QuEChERS protocol, followed by CE-MS/MS analysis. The optimal separation of investigated PFCAs was achieved in less than 9 minutes using 25 mM ammonium acetate buffer and 1 % isopropanol (pH...

A gas chromatography equipped with mass spectrometer (GCMS) method was developed and validated for determination of 16 polycyclic aromatic hydrocarbons (PAHs) in fish using modified quick, easy, cheap, effective, rugged, and safe (QuEChERS) method for extraction and solid phase extraction for sample cleanup to remove most of the coextract combined with GCMS for determination of low concentratio...

Using capillary electrophoresis combined with tandem mass spectrometry, we have developed a method to simultaneously detect lorazepam, clonazepam, temazepam, oxazepam, diazepam, and nitrazepam in urine. The urine samples were submitted to a modified QuEChERS extraction procedure, followed by electrophoretic separation in 0.1 M formic acid electrolyte (pH 2.4) using a polyvinyl alcohol (PVA)-coa...

recently, with increasing public awareness of food safety, developments of some valid and rapidly analytical methods are required for the determination of residual pesticides in crops.this study was conducted on validation of a reliable, accurate and precise method for multi analysis of pesticides residue in melon as a main fruit in iranian food basket. a reliable, and valid method based on spi...

In this study, we sought to assess the applicability of GC-MS/MS for the identification and quantification of 36 pesticides in strawberry from integrated pest management (IPM) and organic farming (OF). Citrate versions of QuEChERS (quick, easy, cheap, effective, rugged and safe) using dispersive solid-phase extraction (d-SPE) and disposable pipette extraction (DPX) for cleanup were compared for...

Rapid and reliable multiresidue analytical methods were developed and validated for the determination of 6 neonicotinoids pesticides (acetamiprid, clothianidin, imidacloprid, nitenpyram, thiacloprid, and thiamethoxam) in honey. A modified QuEChERS method has allowed a very rapid and efficient single-step extraction, while the detection was performed by UHPLC/MS-MS. The recovery studies were car...