Extended X-ray absorption fine structure spectroscopy, mass spectrometry, dynamic light scattering and density functional theory are combined to derive structural models for the interaction of neurotoxicity-ablating platinum-based compounds with the amyloid-β peptide.

Streptomyces showdoensis SANK 65080 produced terferol, an inhibitor of cyclic adenosine 3',5'-monophosphate phosphodiesterase (cAMP-PDE). NMR spectrometry and X-ray analysis were used to determine the structure of the compound, a new member of the terphenyl family.

we report the growth by ion exchange synthesis of zns nanoparticles in mcm-41 matrices using zn (ch3coo)2 and na2s starting sources. the final product (zns/mcm-41) was characterized by x-ray diffraction (xrd) pattern, transmission electron microscopy (tem), scanning electron microscopy (sem), infrared spectrometry (ir) and uv-vis spectroscopy. its crystalline structure and morphology was studie...

polyimide/nickel oxide (polyimide/nio) nanocomposite was successfully synthesized by sol gel technique, using pyromellitic dianhydriede (pmda), 4,4-oxydianiline (oda) and n,n-dimethylacetamide (dmac) and 10 wt% nickel titanate nanopowders (nps). fourier transform infrared spectrometry (ftir), x-ray diffraction (xrd), scanning electron microscopy (sem), and vibrating sample magnetometer (vsm) we...

Natural radionuclides present in soil as well as certain anthropogenic radionuclides released to the environment are the major contributors to terrestrial outdoor exposures. In the assessment of human exposures from environmental radioactivity, besides the conventional method of soil and vegetation sampling combined with laboratory based analyses of environmental media, the other choice would b...

Abstract The Joint Research Centre, in cooperation with the Commissariat à l’Energie Atomique et aux Energies Alternatives, produced a novel 243 Am spike reference material for mass spectrometry. Americium solution an isotopic composition of 88% and 12% 241 was used as source preparation material. certified value 5.696 (11) nmol g −1 amount content 0.136138 (54) n ( Am)/ Am) ratio were assigned...