the effect of mechanical activation on structural changes and kinetics of carbothermic reduction of hematite with graphite was studied in this research. hematite powder mixture with graphite (with stoichiometry ratio c/o=1) was milled for the time periods of zero to 50 hours, and the structural changes were studied using x ray diffraction (xrd). the effect of mechanical activation on the kineti...

Abstract The extent of a chemical reaction has received little attention in the early stages of Chemistry teaching, despite allowing a general way to work with chemical reactions and equilibria. In this article, the concepts of extent of reaction and extent of reaction balances are revised and several applications to study the change in the concentrations of the species involved in chemical rea...

Abstract This work presents attempts to synthesize silver-doped copper nitride nanostructures using chemical solution methods. Copper(II) nitrate and silver(I) were used as precursors the oleylamine a reducing capping agent. Homogeneous Cu 3 N/Ag with diameter of ~ 20 nm obtained in one-pot synthesis by addition copper(II) salt precursor already-synthesized silver nanoparticles (Ag NPs). Synthe...

A novel synthesis of Iimidazo[1,2-c]quinazoline-5(6H)-thione framework was developed through a three-step reaction starting from benzil. The resulting (2-nitrophenyl)-4,5-diphenyl-1H-imidazole  from the reaction of benzil and different 2-nitrobenzaldehyde, reduction of nitro group and then cyclization reaction with carbon disulfide (CS2). All steps were carried out under easy and user-friendly ...

In this research an ultra-fine grained composite structure consisting of an intermetallic matrix together with dispersed nano-sized Al2O3 obtained via mechanical activation of TiO2 and Al in a high energy ball mill and sintering of consolidated samples. Phase composition and morphology of the milled and sintered samples were evaluated by XRD and SEM techniques Thermal behavior of the powder sa...

A one pot green three‐component coupling reaction of aldehyde, phenylacetylene, and amine derivatives in the presence of copper (II)–thioamide combination as a novel and efficient heterogeneous catalyst under solvent–free conditions is reported. The catalyst displayed high activity and afforded the corresponding propargylamines in good to high yields. The key to this procedure was the generatio...

5-Aminosalicylic acid (5-ASA) is currently prepared by electrochemical reduction of 5-nitrosalicylic acid (5-NSA) in acidic media. In this work, electrolytic reduction of 5-NSA in alkaline media is presented. Reactionconditions and parameters such as anode and cathode electrodes, electrolyte type, reaction time, temperature,current, and the pH for isolation of product are investigated. The yiel...

The effect of mechanical activation on structural changes and kinetics of carbothermic reduction of hematite with graphite was studied in this research. Hematite powder mixture with graphite (with stoichiometry ratio C/O=1) was milled for the time periods of zero to 50 hours, and the structural changes were studied using X ray diffraction (XRD). The effect of mechanical activation on the kineti...