A pre-oxidation procedure which converts arsenite [As(III)] into arsenate [As(v)] was investigated in urinary arsenic speciation prior to on-line photo-oxidation hydride generation with ICP-MS detection. This sample pre-oxidation method eliminates As(III) and As(v) preservation concerns and simplifies the chromatographic separation. Four oxidants, Cl2, MnO2, H2O2 and I3-, were investigated. Chl...

Urine can be used to diagnose diabetes in a non-invasively manner. Examination of blood sugar levels as an indicator diabetics is currently carried out using invasive methods. However, most people are not comfortable with the methods used. Early diagnosis non-invasive very important continue developed, including by checking quality urine. This study aims create urine detection based on pH, turb...

BACKGROUND The finding reported in a previous paper - alkalization of urine facilitates uric acid excretion - is contradictory to what one might expect to occur: because food materials for the alkalization of urine contain fewer purine bodies than those for acidification, less uric acid in alkaline urine should have been excreted than in acid urine. To make clear what component of uric acid exc...

We performed 796 dip-stick tests on urine from 100 wild West African chimpanzees (Pan troglodytes verus) from 4 habituated groups in the tropical rain forest of Taï National Park, Cote d'Ivoire, to establish reference values for health monitoring. Specific gravity was also measured on 359 urine samples from 62 chimpanzees. The effect of age, sex, group, month, estrus, pregnancy, meat consumptio...

The formation of various types of kidney stones is strongly influenced by urinary pH. An alkaline pH favors the crystallization of calcium- and phosphate-containing stones, whereas and acidic urine pH promotes uric acid or cystine stones. The activity of many transport processes involved in calcium, citrate and phosphate handling are sensitive to changes in systemic or local pH as shown for sev...

INTRODUCTION: H NMR spectroscopy coupled with pattern recognition methods is being widely used in the classification of biomedical data from biofluids. Urine analysis by NMR is used in the study of inborn errors of metabolism, kidney transplant rejection, urinary tract infection, cancer of organs such as bladder and kidney, and toxicology [1]. There are several experimental conditions that can ...

The Limulus amoebocyte lysate (LAL) test was evaluated for rapid detection of gram-negative bacteriuria in an adult patient population. Time to gelation of a standard LAL preparation was used as a measure of significant (greater than 10(5) bacteria per ml) gram-negative bacteriuria, and the results of 190 LAL assays were compared with quantitative urine cultures. Initially, 33 of 36 urine speci...

The objective of this work was to determine how some wastewater acids could be used to prevent the decomposition of urea into ammonia during storage. The effect of storing human urine with olive oil mill wastewaters (OOMW) or water bubbled with CO2 (BW), was studied. Moreover, the application of two levels of urine dissolved in water OOMW, has been studied in relation to the properties of two s...

A sensitive quantitative method for the determination of matrine alkaloids in human urine was developed based on hollow fiber liquid-phase microextraction (HF-LPME) combined with HPLC. The influence of the different factors on the HF-LPME efficiency including the pH and ion strength of the donar solution, the pH of the acceptor solution, stirring rate and extraction time were examined. The best...