نتایج جستجو برای: 3 c pyrazoles

تعداد نتایج: 2600367  

2008
Jairo Quiroga Jaime Portilla Silvia Cruz Braulio Insuasty Manuel Nogueras Justo Cobo Mike Hursthouse

The solvent-free reaction between 5-amino-1H-pyrazoles and -triketones (2-acetyldimedone and 2acetylindandione) leads to the formation of new fused pyrazolo[1,5-a]pyrimidines in good yields. A possible mechanistic route is postulated on the basis of the isolation of the cyclization intermediate. The structures and regiospecificity of the reaction were determined on the basis of nmr measurements...

2017
Rong Zhou Haiwang Liu Hairong Tao Xingjian Yu Jie Wu

Despite notable recent efforts, a catalytic and convenient strategy for the direct alkylation of unactivated allylic or benzylic sp C–H bonds remains a formidable challenge facing the synthesis community. We herein report an unprecedented allylic/benzylic alkylation using only an organo-photoredox catalyst, which enables coupling of a broad scope of alkenes/arenes and electron-deficient alkenes...

Journal: : 2022

1-Cycloalkyl-2-propene-1-ones were synthesized by electrophilic addition of cycloalkanecarboxylic acid chlorides and its mono- dichloride-substituted derivatives to ethylene in the presence an AlCl3 catalyst at a temperature –10 ÷ –150C dichloroethane medium. The resulting vinyl ketones converted chlorination CCl4 –50C corresponding 1-cycloalkyl-2,3-dichloro-1-propanones, which form 1-R´-3-cycl...

Journal: :Chemical communications 2009
Xin Cheng Shengming Ma

2,3-dihydro-1H-pyrazoles were highly selectively synthesized via the Pd(0)-catalyzed coupling-cyclization reaction of 4-non-substituted 2-substituted 2,3-allenyl hydrazines with aryl iodides in moderate to good yields.

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