نتایج جستجو برای: chromatographic analysis
تعداد نتایج: 2835646 فیلتر نتایج به سال:
In this paper, Artificial Neural Networks are used to solve a complex problem concerning to power transformers and characterized by non-linearity and hard dynamic modeling. The operation conditions and integrity of a power transformer can be detected by analysis of physical-chemical and chromatographic isolating oil, allowing establish procedures for operating and maintaining the equipment. How...
In solution antimony exists either in the pentavalent or trivalent oxidation state. As Sb(III) is more toxic than Sb(V), it is important to be able to perform a quantitative speciation analysis of Sb's oxidation state. The most commonly applied chromatographic methods used for this redox speciation analysis do, however, often show a low chromatographic Sb recovery when samples of environmental ...
The use of derivatization in the analysis of food additivies by chromatographic means has been reviewed. The large majority of these derivatization techniques are employed to facilitate the gas-liquid chromatographic quantitation of various food additives. Silylation, alkylation, acylation, as well as transesterification, saponification, and chemical decomposition techniques are discussed. The ...
We apply matched molecular pair (MMP) analysis to data from ChirBase, which contains literature reports of chromatographic enantioseparations. For the 19 chiral stationary phases we examined, we were able to identify 289 sets of pairs where there is a statistically significant and consistent difference in enantioseparation due to a small chemical change. In many cases these changes highlight en...
For a long time, chromatographic techniques and techniques related to them have stimulated the development of new procedures in the field of pharmaceutical analysis. The newly developed methods, characterized by improved metrological parameters, allow for more accurate testing of, among others, the composition of raw materials, intermediates and final products. The chromatographic techniques al...
From the aerial parts of the endemic species Thymus numidicus Poiret locally which is known as “zaatar”, belongs to the Lamiaceae family five flavonoids were isolated using chromatographic techniques and identified by spectral analysis (UV-Visible, MS, H and CNMR) and chromatographic behaviours.
This work describes a comparative qualitative and quantitative chemical analysis of Maytenus ilicifolia and Maytenus robusta (Celastraceae), extracts by high-resolution gas chromatography (HRGC), using external standards as the method of determination and thin layer chromatographic (TLC). The results show that both plants have a similar chromatographic profile. However, M. robusta exhibited abo...
in this study, a high-performance liquid chromatographic method (hplc) and uv spectrophotometric method were developed, validated and applied for the determination of theophylline in biological fluids. liquid- liquid extraction is performed for isolation of the drug and elimination of plasma and saliva interferences. urine samples were applied without any extraction. the chromatographic separat...
The properties relevant to pharmacokinetics and pharmacodynamics of four series of synthesized s-triazine derivatives have been studied by Quantitative structure-retention relationship (QSRR) approach. The chromatographic behavior of these compounds was investigated by using reversed-phase high performance thin-layer chromatography (RP-HPTLC). Chromatographic retention (RM0) was correlated with...
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