نتایج جستجو برای: hydrothermal process x ray diffraction techniques xrd
تعداد نتایج: 2444415 فیلتر نتایج به سال:
silicon and aluminum sources are most important reactants in the synthesis of zeolite. the use of the silicon source has an important effect on the crystallization of zeolites. also, it can change the properties of the end product. this work reports the influence of three common commercial silica sources such as colloidal silica (ludox am-30), fumed silica and water glass on the crystallinity o...
for several recent years, syntheses of spherical zeolitic materials, such as S-1, ZSM-5 and Beta, have been reported using an anion exchange resin as macro-templates. Conceptually, these syntheses are based on the use of a colloidal crystal templating process. The advantage of this method is preparation of pure self-bonded zeolite micro/macrostructures. In this paper the synthesis of TS-1 is...
The manganese ferrite spinel was synthesized by co-precipitation. The nano sized manganese ferrite characterized by X-ray diffraction (XRD), Scanning electron micrograph (SEM), tunneling electron micrograph (TEM) and Energy dispersive X-ray (EDX) techniques. The adsorption ability of malachite green (MG) from the aqueous solution by manganese ferrite was investigated. It was found that pH value...
The influence of short-time milling on the atomic structure of amorphous Co(70.3)Fe(4.7)B(25) has been investigated by differential scanning calorimetry (DSC), x-ray powder diffraction (XRD), vibrating sample magnetometer (VSM) and x-ray absorption fine-structure (XAFS) techniques. Our results prove that the milling process crystallizes the initially amorphous sample and that the degree of inhe...
Submit Manuscript | http://medcraveonline.com Abbreviations: MB: Methylene Blue; PEC: Photo Electrochemical; Isc: Short Circuit Current; Voc: Open Circuit Voltage; XRD: X-Ray Diffraction; FE-SEM: Field Emission Scanning Electron Microscopy; AOP: Advanced Oxidation Process; CBD: Chemical Bath Deposition; EDS: Energy Dispersive X-Ray Spectroscopy; BET: Brunauer-Emmer-Teller; FWHM: Full Width At H...
Carbon-coated SnO(2) nanorod array directly grown on the substrate has been prepared by a two-step hydrothermal method for anode material of lithium-ion batteries (LIBs). The structural, morphological and electrochemical properties were investigated by means of X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and electrochemical measurement. Wh...
We have been prepared Semiconducting oxide material like TiO2, SiO2, TiO2-SiO2 and TiO2/SiO2 thin films for taken different composition by using hydrothermal method. All these elements were deposited on the glass substrate. In this films are acted on the p and n type working with the majority carrier are recombination of electron and hole .This material is N type but it will acted p-type Ti and...
ZnO-SnO2 hollow spheres were successfully synthesized through a hydrothermal method-combined carbon sphere template. The samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and Fourier transform infrared spectroscopy (FT-IR). The average diameter of hollow spheres is about 150 nm. The photocatalytic activity of the a...
zro2 nanopowder was prepared by the sol-gel auto-combustion method. the product was characterized by x-ray diffraction (xrd), energy dispersive analysis of x-ray (edx) and scanning electron microscopy (sem). the average crystalline size of zro2 was obtained 62 nm. also, photocatalytic removal of nitrophenol from aqueous solution by using nanoscale zro2 under uv light irradiation was studied. th...
Copper orthophosphate, Cu3(PO4)2, and cyclo-tetraphosphates, Cu2P4O12, were synthesized using phosphoric acid and basic copper carbonate, and then treated with a planetary mill for up to 360 minutes. The un-milled and milled samples were characterized by X-ray diffraction (XRD) and Fourier transform infrared (FT-IR) spectroscopy. SEM images, particle size distribution, specific surface area, UV...
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