نتایج جستجو برای: hydrothermal process x ray diffraction techniques xrd

تعداد نتایج: 2444415  

Journal: :journal of chemical and petroleum engineering 0
atieh eskandari faculty of chemical, petroleum and gas engineering, semnan university, semnan, i.r. iran. mansoor anbia research laboratory of nanoporous materials, faculty of chemistry, iran university of science and technology, tehran 16846-13114, iran. mansour jahangiri faculty of chemical, petroleum and gas engineering, semnan university, semnan, i.r. iran. fariba mohammadi nejati faculty of chemical, petroleum and gas engineering, semnan university, semnan, i.r. iran.

silicon and aluminum sources are most important reactants in the synthesis of zeolite. the use of the silicon source has an important effect on the crystallization of zeolites. also, it can change the properties of the end product. this work reports the influence of three common commercial silica sources such as colloidal silica (ludox am-30), fumed silica and water glass on the crystallinity o...

آقابزرگ, حمید رضا, بنکدار سخی, راضیه , صالحی راد, فتح الله ,

for several recent years, syntheses of spherical zeolitic materials, such as S-1, ZSM-5 and Beta, have been reported using an anion exchange resin as macro-templates. Conceptually, these syntheses are based on the use of a colloidal crystal templating process. The advantage of this method is preparation of pure self-bonded zeolite micro/macrostructures. In this paper the synthesis of TS-1 is...

2015
SAEEDEH HASHEMIAN

The manganese ferrite spinel was synthesized by co-precipitation. The nano sized manganese ferrite characterized by X-ray diffraction (XRD), Scanning electron micrograph (SEM), tunneling electron micrograph (TEM) and Energy dispersive X-ray (EDX) techniques. The adsorption ability of malachite green (MG) from the aqueous solution by manganese ferrite was investigated. It was found that pH value...

Journal: :Journal of physics. Condensed matter : an Institute of Physics journal 2007
K Saksl J Bednarčík R Nicula E Burkel S Roth H Franz

The influence of short-time milling on the atomic structure of amorphous Co(70.3)Fe(4.7)B(25) has been investigated by differential scanning calorimetry (DSC), x-ray powder diffraction (XRD), vibrating sample magnetometer (VSM) and x-ray absorption fine-structure (XAFS) techniques. Our results prove that the milling process crystallizes the initially amorphous sample and that the degree of inhe...

2017

Submit Manuscript | http://medcraveonline.com Abbreviations: MB: Methylene Blue; PEC: Photo Electrochemical; Isc: Short Circuit Current; Voc: Open Circuit Voltage; XRD: X-Ray Diffraction; FE-SEM: Field Emission Scanning Electron Microscopy; AOP: Advanced Oxidation Process; CBD: Chemical Bath Deposition; EDS: Energy Dispersive X-Ray Spectroscopy; BET: Brunauer-Emmer-Teller; FWHM: Full Width At H...

2010
Xiaoxu Ji Xintang Huang Jinping Liu Jian Jiang Xin Li Ruimin Ding Yingying Hu Fei Wu Qiang Li

Carbon-coated SnO(2) nanorod array directly grown on the substrate has been prepared by a two-step hydrothermal method for anode material of lithium-ion batteries (LIBs). The structural, morphological and electrochemical properties were investigated by means of X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and electrochemical measurement. Wh...

2013
C. Gopinathan M. Kavitha

We have been prepared Semiconducting oxide material like TiO2, SiO2, TiO2-SiO2 and TiO2/SiO2 thin films for taken different composition by using hydrothermal method. All these elements were deposited on the glass substrate. In this films are acted on the p and n type working with the majority carrier are recombination of electron and hole .This material is N type but it will acted p-type Ti and...

2016
Changqing Jin Chenghai Ge Zengyun Jian Yongxing Wei

ZnO-SnO2 hollow spheres were successfully synthesized through a hydrothermal method-combined carbon sphere template. The samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and Fourier transform infrared spectroscopy (FT-IR). The average diameter of hollow spheres is about 150 nm. The photocatalytic activity of the a...

Journal: :international journal of nano dimension 0
a. a. mehrdad sharif department of analytical chemistry, faculty of chemistry, north tehran branch, islamic azad university, tehran, iran. s. abedini khorrami department of analytical chemistry, faculty of chemistry, north tehran branch, islamic azad university, tehran, iran. n. assi department of analytical chemistry, faculty of chemistry, north tehran branch, islamic azad university, tehran, iran.

zro2 nanopowder was prepared by the sol-gel auto-combustion method. the product was characterized by x-ray diffraction (xrd), energy dispersive analysis of x-ray (edx) and scanning electron microscopy (sem). the average crystalline size of zro2 was obtained 62 nm. also, photocatalytic removal of nitrophenol from aqueous solution by using nanoscale zro2 under uv light irradiation was studied. th...

2009
Hiroaki Onoda Ken-ichi Okumoto Atsushi Nakahira Isao Tanaka

Copper orthophosphate, Cu3(PO4)2, and cyclo-tetraphosphates, Cu2P4O12, were synthesized using phosphoric acid and basic copper carbonate, and then treated with a planetary mill for up to 360 minutes. The un-milled and milled samples were characterized by X-ray diffraction (XRD) and Fourier transform infrared (FT-IR) spectroscopy. SEM images, particle size distribution, specific surface area, UV...

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