نتایج جستجو برای: nanocrystalline powder
تعداد نتایج: 56786 فیلتر نتایج به سال:
Background: CdWO4 is a scintillator with some unique properties. For example, high density, thermal and chemical stability and so on. Different applications of this scintillator such as X-ray scintillator has been investigated thoroughly so far. However, there is limited number of studies reporting the characteristics of CdWO4 as an alpha counter. Materials and Methods: The CdWO4 powder was syn...
Nanoscale potassium niobate (KNbO3) powders of orthorhombic structure were synthesized using the sol-gel method. The heat-treatment temperature of the gels had a pronounced effect on KNbO3 particle size and morphology. Field emission scanning electron microscopy and transmission electron microscopy were used to determine particle size and morphology. The average KNbO3 grain size was estimated t...
A chemical and a physical method have been applied for the preparation of chromium-nickel alloy nanoparticles. These particles were designed to be used for controlled magnetic hyperthermia applications. Microemulsions with Ni2+ and Cr3+ and/or NaBH4 as precursors were prepared using the isooctane/CTAB, n-butanol/H2O system. The samples of CrxNi1-x nanoparticles with the desired composition were...
Using a combination of high resolution X-ray powder diffraction and X-ray Raman scattering spectroscopy at the B K- and Ca L2,3-edges, we analyzed the reaction products of Ca(BH4)2 after annealing at 350 °C and 400 °C under vacuum conditions. We observed the formation of nanocrystalline/amorphous CaB6 mainly and found only small contributions from amorphous B for annealing times larger than 2 h...
low water-wettability and oxidation resistance of graphite have limited its application in carbon containing refractory castables. the aims of this study were improvement of water-wettability and the oxidation resistance of natural flaky graphite by applying an oxide coating on its surface. to develop the coating, magnesium aluminate spinel sol was formulated via a citrate-nitrate route and gra...
in this study, a feasible green method for the synthesis of copper oxide nanocrystalline is described by using sour cherry juice which has a significant effect on crystalline size, and morphology. the benefits of the green method, not only nanometer scale are formed but also low-cost method are obtained in a normal atmosphere which it has been used (ch3coo)2cu.h2o individually as cu sources. al...
production of fe-c alloy powders by mechanical alloying was studied. fe and graphite elemental powdermixtures containing 0.8 and 1.5wt.% graphite were mechanically alloyed using a planetary ball mill. thestructural changes of powder particles during mechanical alloying were studied by x-ray diffractometery,scanning electron microscopy and microhardness measurements. for both compositions, mecha...
In this work TiNi-based nanocrystalline alloys and composite were produced by mechanical alloying process with subsequent annealing at 750 ◦C for 0.5 h. Mechanical alloying was performed in a SPEX 8000 Mixer Mill. TiNi alloy was chemically modi ed by Ag elemental powder. Silver content equaled 5 wt%. X-ray di raction analyses revealed formation of TiNi main phase after annealing. Additionally, ...
A modified solution combustion approach was used for the first time in the preparation of nanosize zirconia toughened alumina (ZTA) composite. ZTA-1 with an average particle size of 37 nm was prepared using corresponding metal nitrates and urea. ZTA-2 with an average particle size of <10 nm was prepared by using mixture of fuels such as ammonium acetate, urea and glycine. The products formed we...
In this study, nanocrystalline cellulose (NCC) was used for increasing the bonding strength of urea-formaldehyde (UF) resin adhesive, with a reduction of formaldehyde (HCHO) emissions. The surface of NCC was modified by 3-aminpropyltriethoxysilane (APTES) and 3-methacryloxypropyltrimethoxysilane (MPS) for the lack of compatibility with UF resin adhesive. The modified NCC was characterized by X-...
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