The developserit, by collaborative study, of a standardised metbod for the determination of the canponent triglycerides of animal and vegetable oils and fats is described. The procedure involves the separation of the triglycerides into groups containing the same number of carbon atoms, the separation being achieved by direct gas-liquid chranatograiy of solutions of the lipids on packed columns ...

The title compound, C(16)H(21)BO(6), has has approximate C(2) symmetry, but no crystallographically imposed mol-ecular symmetry. In the crystal, mol-ecules are packed into parallel columns along the a axis. Short inter-molecular C-H⋯O contacts stabilize the crystal packing.

some formation, such as " single column," or " double column," or " column of fours," according as the width of the road, and nature of the ground permitted. Any one who has been on active service with Indian Field Hospitals and Bearer Columns, must have observed the want of order that prevails, and how the men straggle all over the line of march. I think that all the men of the A. H. N. C. sho...

The goal of this study was to evaluate the accuracy of simulated robustness testing using commercial modelling software (DryLab) and state-of-the-art stationary phases. For this purpose, a mixture of amlodipine and its seven related impurities was analyzed on short narrow bore columns (50×2.1mm, packed with sub-2μm particles) providing short analysis times. The performance of commercial modelli...

In the title mol-ecule, C(16)H(13)Cl O(3), the two aromatic rings form a dihedral angle of 65.3 (1)°. In the crystal structure, weak inter-molecular C-H⋯O hydrogen bonds link the mol-ecules into centrosymmetric dimers, which are further packed into columns propagating in [100] by weak C-H⋯π inter-actions.

Equations developed for packed columns may be used to predict the overall heat transfer coefficient and friction loss in massecuite reheaters. The results seem to indicate that exchangers with the tubes staggered give higher heat transfer rates than those with the tubes in line.

In this study molecular imprinting technology was employed to prepare a specific affinity sorbent for the resolution of Methylephedrine, a chiral drug. The molecularly imprinted polymer (MIP) was prepared by non-covalent molecular imprinting with either (+) or (-)-Methylephedrine ((R*,S*)-2-(methylamino)-1phenylpropan-1-ol) as the template. Methacrylic acid and ethylene glycol di-methacrylate w...

Over the years, separation resolution and reduction of analysis time has continually improved in High Performance Liquid Chromatography (HPLC). For further improvement, column efficiency must be increased. The relationship among separation efficiency, the mobile phase linear velocity and particle size was investigated in detail in the early 1970 s [1]. This and other systematic investigations h...

Optimisation of peak capacity is an important strategy in gradient liquid chromatography (LC). This can be achieved by using either long columns or columns packed with small particles. Monolithic columns allow the use of long columns at relatively low back-pressure. The gain in peak capacity using long columns was evaluated by the separation of a tryptic bovine serum albumin digest with an LC-U...