The hot deformation behavior and microstructural evolution of an Al-Zn-Mg-Cu (7150) alloy was studied during hot compression at various temperatures (300 to 450 °C) and strain rates (0.001 to 10 s-1). A decline ratio map of flow stresses was proposed and divided into five deformation domains, in which the flow stress behavior was correlated with different microstructures and dynamic softening m...

Physical properties of commercial carbamazepine (CBZ) samples can significantly influence drug release and thereby jeopardize bioequivalence of the final dosage form. The aim of this study was to reduce variability in commercial CBZ samples by recrystallization. CBZ samples of four different suppliers were recrystallized in ethanol solution containing 1% polyvinylpyrrolidone (PVP). CBZ samples ...

Copper bonding wires were characterized using electron backscatter diffraction (EBSD). During drawing, shear components are mainly located under the surface and ,111. and ,100. fiber texture components develop with similar volume fractions. Grain average misorientation (GAM) and scalar orientation spread (SOS) of the ,100. component are lower than those of the ,111. or other orientations. Also,...

Selective sulfoxidation of BEDT-TTF (bis(ethylenedithio)-tetrathiafulvalene) with enantiopure (camphoryl-sulfonyl)oxaziridine derivatives provided the inner monosulfoxide, as demonstrated using single crystal X-ray analysis, with an enantiomeric excess of 44% (up to 74% after recrystallization).

Alloisoleucine, prepared from a mixture of racemic isoleucine-alloisoleucine diastereoisomers, can be heavily contaminated with isoleucine if the recrystallization of acetyl-dl-alloisoleucine is controlled by melting point only. Two commercial specimens were found to be thus contaminated.

The evolution of texture as a function of recrystallization has been characterized for hotrolled AA1050. Samples prepared from hot rolled sheet were annealed isothermally for sufficient time to allow complete recrystallization. The microstructural variation and texture evolution in the samples was observed by automatic indexing of Electron Back Scatter Diffraction (EBSD) patterns in a Scanning ...

Purpose: To establish an efficient method to recycle natural borneol from Cinnamomum camphor chvar. Borneol oil residue. Methods: The fractions and raffinate of the oil residue of Cinnamomum camphor chvar. Borneol were obtained by fractional distillation, and analyzed by gas chromatography with flame ionization detector (GC-FID) and gas chromatographymass spectrometry (GC-MS). Natural borneol w...