نتایج جستجو برای: sba 15 pr so3h
تعداد نتایج: 526550 فیلتر نتایج به سال:
We report the first synthesis of titanium nitride (TiN) nanoparticles inside the nanoscale channels of mesoporous silica SBA-15. The TiN precursor, Ti(NMe(2))(4) in toluene, was incorporated into the methyl group-modified channels of the SBA-15 powder. The functionalization of pore surfaces with methyl groups generates hydrophobic surfaces that facilitate impregnation with Ti(NMe(2))(4) and min...
Mesoporous silica, SBA-15 was successfully functionalized with quinoline moiety, and was applied as a matrix in the MALDI-TOF-MS analysis of small molecules. The modified SBA-15 material [SBA-15-8-(3-(triethoxysilyl)propoxy) quinoline, SBA-15-8QSi] was obtained by using calcined SBA-15 and 8-hydroxy quinoline. The structure of the functionalized mesoporous material was systemically characterize...
The mechanism for the controlled synthesis of highly dispersed vanadia supported on mesoporous silica SBA-15 (VOx/SBA-15) is elucidated using X-ray photoelectron spectroscopy (XPS), Raman and diffuse reflectance infrared Fourier-transform spectroscopy (DRIFTS). The synthesis consists of functionalization of SBA-15 using 3-aminopropyltrimethoxysilane (APTMS) followed by HCl treatment, anion exch...
Pt nanoparticles with controlled sizes between 1.6–7.0 nm were anchored onto the surface and pores of SBA-15 silica support. The catalysts were characterized by TEM-ED, BET, XRD, and ICP-MS techniques and were tested in liquid phase hydrosilylation of phenylacetylene with triethylsilane. The activity of the 7.0 nm Pt nanoparticles anchored onto the surface of SBA-15 in hydrosilylation (TOF = 0....
Under pH 7 - 10 conditions, the mesoporous silica supports proposed for use in water treatment are relatively unstable. In batch experiments conducted in pH 7 solutions, the commonly used support SBA-15 dissolved quickly, releasing approximately 30 mg/L of dissolved silica after 2 hours. In column experiments, more than 45% of an initial mass of 0.25 g SBA-15 dissolved within 2 days when a pH 8...
A kind of mesoporous hybrid luminescence material was assembled through the ion exchange method between [Ln(DPA)3](3-) and ionic liquid functionalized SBA-15. [Ln(DPA)3](3-) was successfully anchored onto positive-charge modified SBA-15 by the strong electrostatic interaction. In [Ln(DPA)3](3-), Ln(3+) ions are in 9-fold coordination through six oxygen atoms of carboxyl groups and three nitroge...
We studied the effect of two types of mesoporous silica nanoparticles, MCM-41 and SBA-15, on mitochondrial O 2 consumption (respiration) in HL-60 (myeloid) cells, Jurkat (lymphoid) cells, and isolated mitochondria. SBA-15 inhibited cellular respiration at 25-500 microg/mL; the inhibition was concentration-dependent and time-dependent. The cellular ATP profile paralleled that of respiration. MCM...
این پروژه شامل پنج قسمت به شرح زیر انجام و توضیح داده می شود: قسمت اول مربوط به استخراج سیلیس از خاکستر ساقه جارو است و آنالیز طیفی آن با xrf،xrd، ir)-ft) انجام شد. قسمت دوم مربوط به سنتز نانو بلورهای زئولیت سیلیکاتی sba-15 با استفاده از ماده طاق ساز آلی در اندازه نانومتری می باشد. sba-15یکی از مواد مزو متخلخل است که به دلیل داشتن ویژگیهای منحصر به فردی همچون سطح ویژه بالا، حفرات بزرگ و سطح ...
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