The synthesis of CaCO3/Cu2O/GO nanocomposites was developed by sol-gel auto-combustion method. analysis structure completed on X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), Raman spectroscopy, and environmental scanning electron microscopy (ESEM). XRD spectra the matched crystal CaCO3/Cu2O. average size 20 nm for Cu2O 25 CaCO3 nanoparticles. FTIR data showed absorptio...

The complete oxidation of n-Hexane and iso-Octane was studied individually in a fixed bed tubular flow reactor over CuO-CeO2 catalysts synthesized via four different methods namely urea-nitrate combustion method, urea gelation/co-precipitation method, citric acid sol-gel method and co-impregnation method. Laser diffraction was employed in catalysts characterization. The results obtained from th...

Spinel ferrite nanocomposites of Ni1–xZnxFe2O4 (x = 0.25 and 0.75) were synthesized by sol-gel auto-combustion annealed between 250°C 1000°C. A single-phase spinel structure was found through X-ray diffraction (XRD). The crystallite size is in the range 17.55–66.98 nm, lattice parameters are 8.351–8.434 Å. analysis revealed a slight shift peaks towards shorter angles when zinc concentration inc...

structural properties and chemical composition change the photocatalytic activity in tio2-sio2 nanopowder composite. the sio2-tio2 nanostructure is synthesized based on sol–gel method. the nanoparticles are characterized by x-ray fluorescents (xrf), x- ray diffraction (xrd), tunneling electron microscopy (tem), field emission scanning electron microscopy (fe-sem), uv-vis. spectrophotometer and ...

in order to improve uv and visible lights photocatalytic activities of the pure anatase tio2, a novel and efficient n-doped tio2 photocatalyst was prepared by sol-gel method. n-doped titania is prepared using triethylamine (with difference molar ratios) as the nitrogen source. the crystalline structure, morphology, particle size, absorbance and band-gap and chemical structure of n-doped tio2 wa...

the silica supported platinum nanoparticles was synthesized by using the sol-gel method. the possibility of using diamminedinitro platinum (ii) as pt precursor and effect of metal precursor concentration on the final pt nanoparticle size was investigated. a stable silica sol was prepared via hydrolysis of tetraethyl orthosilicate (teos) as a metal alcoxide and condensation reaction. subsequentl...

highly crystalline bi3+-doped cadmium oxide (cdo) sub-micron structures were synthesized by calcination the obtained precursor from a sol-gel reaction. the reaction was carried out with cadmium nitrate (cd(no3)2.4h2o), bismuth nitrate (bi(no3)3.5h2o) and ethylene glycol (c2h6o2) reactants without any additives at 80°c for 2h. resulting gel was calcined at 900 °c with increasing temperature rate...

nano structured materials have wide range of applications due to their interesting size-dependent chemical and physical properties compared to particles of size in the range of micrometer. copper oxide nano materials are of interest on account of their potential uses in many technological fields. in this study  cuo nanoparticles were synthesized via simple sol gel method using basic cuso4 as we...