This work is focused on synthesis of SiO2- CNT hybrides via sol-gel method. Homogeneous distribution of carbon nanotubes within silicon matrix was obtained by mixing the functionalized carbon nanotube (CNTCOOH) with active silicic acid followed by titration to the solution of sodium silicate (Na2SiO3) under the average temperature condition of 80?C. Different ratios of multi-walled carbon nanot...

In this research, synthesis and characterization of silver/alumina composite powders was investigated. This kind of metal/ceramic composite powders is used for fabrication of cutting tools inserts. The role of silver is toughening the final product. The powders were synthesized via co-precipitation method. The composition of the synthesized powders was Ag/80% wt 〖Al〗_2 O_3. Silver nitrate, alum...

An overview of the synthesis and applications of chiral 2,3-epoxy alcohols containing unsaturated chains is presented. One of the fundamental synthetic routes to these compounds is Sharpless asymmetric epoxidation, which is reliable, highly chemoselective and enables easy prediction of the product enantioselectivity. Thus, unsaturated epoxy alcohols are readily obtained by selective oxidation o...

Peptidoglycan precursors containing D-Cys at position 4 were polymerised to form a synthetic peptidoglycan layer, which could be fluorescently labelled, providing a new method to monitor peptidoglycan transglycosylation and transpeptidation.

α-Bromoketals and acetals are important synthetic precursors in organic synthesis. In this work, some new α-bromoketals are synthesized by the reaction of aryl methyl ketones with diols in the presence of 1,8-diazabicyclo[5.4.0] undec-7-ene (DBU) hydrobromide-perbromide in good isolated yields. The latter compound converts aldehydes to acetals and serves as a new and efficient reagent for t...

Neurosteroids are steroids that are produced in the central nervous system (CNS). While progesterone and dehydroepiandostendione (the precursors of testosterone) are among the identified neurosteroids, it is not clear that testosterone could be considered as a neurosteroid. The testosterone synthesis has been demonstrated in the brain of castrated frog, but not in the rat brain. In the present ...

Because of the importance of microbial metabolites of cholesterol as precursors in the synthesis of steroidal drugs, we decided to study the ability of Arthrobacter simplex to degrade cholesterol. Arthrobacter simplex cleaves the side chain of cholesterol in the presence of 2,2'-dipyridyl and produces 4-androstene-3,17- dione (AD) and androsta- 1,4-diene-3,17-dione(ADD). Two other intermedi...

CuAlS2  Chalcopyrite  nanocrystalline  are  synthesized  with  facile method.  The  heat  arrested  solvothermal  method  for  synthesize nanocrystalline  were  investigated.  The  time  duration  of  synthesis, temperature of solution and metal salts to solvent molar ratio can be parameters  that we are  studied. The nanoparticles were  synthesized with CuCl, AlCl3 and  thiourea (SC(NH2)2...

This study reports the simple process to synthesis of CuO/CuI nanocomposite in a non-aqueous solution. In the conducted experiments CuI and Dimethyl Sulfoxide (DMSO) were used as the precursors. Moreover, DMSO had role of solvent and ligand simultaneously. In experiments the effects of oleic acid as the particles size modifier, temperature and concentration were investigated. Crystalline struct...