this paper describes day-one beamlines of the iranian light source facility and design concept of powder diffraction and spectromicroscopy beamlines as the most priorities of each synchrotron that cover the research requirements in the fields of physics, chemistry, nano-science, etc. for powder diffraction beamline energy range is 6-30 kev, resolution: 10-4, flux: 1012(ph/s/0.1%b.w.) and spot s...

Tungsten tetraboride (WB(4)) is an interesting candidate as a less expensive member of the growing group of superhard transition metal borides. WB(4) was successfully synthesized by arc melting from the elements. Characterization using powder X-ray diffraction (XRD) and energy-dispersive X-ray spectroscopy (EDX) indicates that the as-synthesized material is phase pure. The zero-pressure bulk mo...

PURPOSE The knowledge of the mechanical response of bones and their substitutes is pertinent to numerous medical problems. Understanding the effects of mechanical influence on the body is the first step toward developing innovative treatment and rehabilitation concepts for orthopedic disorders. METHODS This was a comparative study of 5 synthetic scaffolds based on porous calcium phosphates an...

the silica aerogel was prepared by the acid–base sol–gel polymerization of tetraethylorthosilicate precursor followed by ambient pressure drying. the prepared silica aerogels were characterized by fourier transform infrared )ft-ir(, thermo-gravimetric and differential thermal analysis )tg/dta(, x-ray diffractometer )xrd(, energy dispersive x-ray microanalysis )edx(, brunauer–emmitt–teller (bet)...

in this research, cuo spherical-like nanoparticles were synthesized using the planetary ball mill method. the structure, particle size and morphology of the resulting cuo nanoparticles were characterized by xrd (x-ray diffraction), sem (scanning electron microscopy) and saxs (small-angle x-ray scattering) methods. the results of this investigation showed that the smallest particles which were o...

This research developed new nanostructured Al–Fe3O4 composites via accumulative roll bonding (ARB). X-ray diffraction (XRD) analysis and field emission scanning electron microscopy were conducted to examine microstructural characteristics and particle distribution in the nanocomposites. Hardness and tensile strength tests were employed to examine their mechanical propertie...

zns  nanoparticles  were  synthesized  via  a  simple  surfactant  free microwave  route.  in  this  synthesis, thioacetamide  was  used  as sulfur  source.  the effects  of different  parameters  such  as  type of zinc precursor,  time  and  power  of  irradiation  on  the  morphology and  particle  size  of  the  products  have been  investigated.  the nanostructures  were  characterized  by ...

in this study, physical vapor deposition (pvd) ti-cr-n coatings were deposited at two different temperatures100 and 400ºc on hardened and tempered tool steel substrates. the influence of the applied deposition temperature on the physical and mechanical properties of coatings such as roughness, thickness, phase composition, hardness and young’s modulus were evaluated. phase compositions were stu...

In this investigation, MoSx/Cr coatings were deposited by direct-current magnetron sputter onto Ck45 (AISI 1045) plain carbon steel substrates. The MoSx/Cr ratio in the coatings was controlled by sputtering the composite targets. The chemical characterization was performed using EDX (energy dispersive X-ray analysis); the structural characterization was accomplished by X-ray diffraction (XRD) s...