We present a supercritical CO 2 (SCCO 2) process for the preparation of nanoporous organosilicate thin films for ultra low dielectric constant materials. The porous structure was generated by SCCO 2 extraction of a sacrificial poly(propylene glycol) (PPG) from a nanohybrid film, where the nanoscopic domains of PPG porogen are entrapped within the crosslinked poly(methylsilsesquioxane) (PMSSQ) m...

A multiresidue quantitative screening method covering 39 antibiotics from 7 different families by ultra-high-pressure-liquid-chromatography-tandem mass spectrometry (UHPLC-MS/MS) is described. Sulfonamides, trimethoprim, tetracyclines, macrolides, quinolones, penicillins and chloramphenicol are simultaneously detected in liver tissue. A simple sample treatment method consisting of extraction wi...

A new micell-mediated phase separation method for preconcentration of ultra-trace quantities of cadmium as a prior step to its determination by flame atomic absorption spectrometry has been developed. The method is based on the cloud point extraction (CPE) of cadmium in iodide media with Triton X-114 in the absence of any chelating agent. The optimal extraction and reaction conditions (e.g., ac...

purpose the aims of the present study were to investigate (i) the changes in participation and performance and (ii) the gender difference in triple iron ultra-triathlon (11.4 km swimming, 540 km cycling and 126.6 km running) across years from 1988 to 2011. methods for the cross-sectional data analysis, the association between with overall race times and split times was investigated using simple...

background: the possible role of cochlear function in tinnitus generation is still a matter of debate. to assess the role of outer hair cell dysfunction in tinnitus and its possible relationship with ultra-high frequency (uhf) hearing sensitivity, transient evoked otoacoustic emissions (teoae) and uhf hearing thresholds were investigated in normal hearing individuals with and without tinnitus. ...

regarding many disadvantages of traditional method to produce concentrated yoghurt, several attempts have been done for mechanization of process in industrial scale. using membrane systems especially ultra filtration is one of these methods. in this survey, method to produce direct concentrated yoghurt, fresh milk was concentrated to 19% snf by ultra filtration method then diluted to 13 and 16 ...

objective: to compare the outcome of patients with up to 60% total body surface area (tbsa) thermal burns undergoing ultra-early and early excision and grafting. methods: this historical cohort study was performed in two referral burn centers of shiraz during a 1-year period from 2015 to 2016. we included those patients with thermal burns up to 60% tbsa who underwent ultra-early (48-72 hours) a...

the ultra-nanocrystalline diamond (uncd) was synthesized by the detonation of a high explosive mixture in water confinement. the presence of a diamond phase was revealed by x-ray diffraction (xrd) and transmission electron microscopy (tem). x-ray line broadening (xrlb) was used to evaluate the peak profiles of diamond nanoparticles and their corresponding average crystallite sizes. the micro st...

The tandem mass spectrum extraction of phosphopeptides is more difficult and error-prone than that of unmodified peptides due to their lower abundance, lower ionization efficiency, the cofragmentation with other high-abundance peptides, and the use of MS(3) on MS(2) fragments with neutral losses. However, there are still no established methods to evaluate its correctness. Here we propose to ide...