This paper describes thermoelectric properties of La-doped SrTiO3 prepared by using a combination of combustion synthesis (CS) with post spark plasma sintering (SPS), on which effects of sintering temperature were mainly examined. In experimental, combustion-synthesized (CSed) samples (Sr1 xLaxTiO3, x 1⁄4 0:08) were spark-plasma-sintered (SPSed) at temperatures from 1513 to 1663K and the thermo...

the fuel cells are distinguished as generating of green allocable energy and are electrochemical devices of low environmental impact. porous nanocrystalline strontium-doped lanthanum manganite la0.8sr0.2mno3 (lsm) cathode materials were prepared by mechanochemical route in various grinding times. carbon black was employed to produce pores. the formation of lsm single phase was studied by x-ray ...

In the present paper the sintering behavior of 3 mol% yttria-stabilized zirconia (3Y-TZP) with and without small amount (0.2 wt %) of SiO2 additive was investigated. It has been studied the silica impact which was added in two ways (co-precipitation and mechanical mixing) on sintering kinetics of 3Y-TZP nanopowders at the initial sintering stage. It was found the silica additive leads to the ch...

Zr1−xTixC (x = 0, 0.2, 0.4, 0.6, 0.8, 1) solid solution ceramics were fabricated by flash spark plasma sintering (FSPS). The phase composition, microstructure, and mechanical property of the sintered investigated. results showed that composition plays a key role on densification ceramics. A high relative density (98.6 %) hardness (>20 GPa) was achieved in Zr0.4Ti0.6C. unique in-situ temperature...

The apparent activation energy of sintering for 8-mol%-Y2O3-doped ZrO2 during shrinkage-rate-controlled flash was determined using a master curve. SCF found to decrease from approximately 700 430 kJ/mol with density. in high-density region is similar value lattice diffusion, 460 kJ/mol. relative density range over which the occurred smaller than thermal and further moved lower temperature range...

Nanoparticles have been an area of active research in recent years due to their properties, which can be greatly different from the bulk. In this work, we study the sintering of TiO2 nanoparticles using molecular dynamics simulations. Such sintering occurs in flame reactors where nanotitania is prepared via the chloride process. Decrease in free energy due to reduction in surface area is the ma...

In this study, synchrotron radiation computed tomography was applied to investigate the mechanisms of titanium powder microwave sintering in situ. On the basis of reconstructed images, we observed that the sintering described in this study differs from conventional sintering in terms of particle smoothing, rounding, and short-term growth. Contacted particles were also isolated. The kinetic curv...

The laser sintering process of multi-component powder W/Cu is simulated by ANSYS software based on the factors of radiation, convection and thermal physical parameters on temperature. The laser power and scanning velocity which are the key process parameters to affect directly in sintering molding are studied in paper. The results show that when the scanning velocity is constant, the sintering ...

Until 2000 almost all research in the microwave sintering area was confined to non-metallic materials. However, after the first report by Penn State in 1999 on full sintering of steel powders in microwave, now in the last few years there has been increasing interest in applying microwave energy for processing of variety of metallic materials. The present study is an extension of this work and r...