Connections with a local mental health service for young people, headspace, led to collaboration between local health service dietitian’s and headspace staff. This partnership enables early detection and treatment of young people with disordered eating in Tamworth NSW. A project identified the need to enhance staff awareness of nutrition and disordered eating, improved management of young peopl...

Production of high value products from glycerol via anaerobic fermentation is of utmost importance for the biodiesel industry. The microorganism Escherichia coli (E. coli) K12 was used for fermentation of glycerol. The effects of glycerol concentration and headspace conditions on the cell growth, ethanol and hydrogen production were investigated. A full factorial experimental design with 3 repl...

A new MIMS-derived technique, headspace membrane introduction mass spectrometry (HS-MIMS), is described for direct trace level analysis of volatile organic compounds (VOCs) in soil and other dry or wet solid matrixes. A silicone membrane interface is placed about 15 cm from the ion source, and a closed airspace (headspace) is created by connecting a toggle valve to the 1/4 in. tubing that conne...

The carbon-isotopic composition (delta13C) of soil-respired CO2 has been employed to evaluate soil carbon-cycling processes and the contribution of soil CO2 emissions to canopy and tropospheric air. These evaluations can be successful only when accurate isotope values of soil-respired CO2 are available. Here, we tested the robustness of delta13C values of soil-respired CO2 obtained after long i...

In this paper, a chromatographic method for the determination of volatile organic compounds (VOCs) as tool Gram-positive and Gram-negative bacterial strains identification was described. Direct Headspace gas chromatography coupled with mass spectrometry (Headspace-GC-MS) has been used qualitative VOCs emitted by certain (Salmonella Typhimurium, Escherichia coli, Serratia rubidae, Staphyloccocus...

When fermentation research requires the comparison of many strains or conditions, major bottleneck is a technical one. Microplate approaches are not able to produce representative fermentative performance due their inability truly operate anaerobically, whilst more traditional methods do facilitate sample density sufficient assess enough candidates be considered even medium throughput. Two robo...

Petroleum products and essential oils are produced used in large amounts categorized as Substances of Unknown or Variable composition, Complex reaction Biological materials (UVCBs). These UVCBs notorious difficult-to-test substances, since they complex mixtures hydrophobic volatile compounds. This study introduces two passive dosing (PD) approaches for whole UVCB toxicity testing: (1) headspace...

Volatile compounds in honey samples of different botanical origins were investigated. Solid phase microextraction (SPME) and gas chromatography-mass spectrometry (GC/MS) revealed a total of 86 compounds in the headspace of 4 types of honey – multifloral, heather, buckwheat and lime-honeydew. The chemical composition of the headspace was very diverse, owing to the presence of compounds from diff...

A method for optimization of extraction of volatile compounds in Chardonnay wine was developed using headspace-solid phase microextraction (HS-SPME) and gas chromatography coupled with triple quadrupole tandem mass spectrometry (GCMS/MS). Optimization of the HS-SPME conditions, temperature (T, ̊C) and extraction time (t, minutes), was carried out using a 2 factorial central composite rotational...

An analytical method for the quantification of residual solvents in annatto extracts, natural food colorants, was established using a static headspace gas chromatography (HSGC) coupled with a flame ionization detector (FID). As a sample diluent in a headspace sampling, dimethylformamide (DMF) was selected owing to its high capacity for dissolving both bixin-based and norbixin-based annatto extr...