ABSTRACT: A combined gas chromatography-mass spectrometry (GC-MS) with headspace solid-phase micro extraction (SPME) method has been employed for the analysis of the flavor volatiles of three different rice cultivar, including two modified Iranian rice cultivars and Hashemi rice cultivar during gelatinization. The proposed combination provided a powerful system for easy and rapid screening of a...

A headspace-solid phase microextraction (HS-SPME) and gas chromatography-mass spectrometry (GC-MS) method has been developed for the simultaneously determination of 20 disinfection by-products (DBPs) in water samples from reverse osmosis (RO) membranes. Selected compounds belong to different families including: trihalomethanes (THMs), halogenated acetonitriles (HANs), halogenated nitromethanes ...

Solid phase microextraction (SPME) is a popular sampling technique whereby analytes are sorbed to a coated fiber and subsequently desorbed into an analytical instrument. In headspace SPME, analytes partition between the sample, the headspace above the sample, and the SPME fiber coating. In total vaporization SPME (TV-SPME), sample extracts are heated until both the solvent and analytes complete...

Litsea cubeba L., also named as Makauy, is a traditional herb and has been used as cooking condiment or tea brewing to treat diseases for aborigines. The present study was undertaken to explore the chemical compositions of the fruit essential oil of L. cubeba (LCEO) and the immunomodulatory effect of LCEO on dendritic cells and mice. The LCEO was analyzed using gas chromatography (GC) and gas c...

The effect of solvent polarity (methanol and pentane) on the chemical composition of hydrodistilled essential oils (EO's) of Lippia graveolens H.B.K. (MXO) and Origanum vulgare L. (EUO) was studied by GC-MS. Composition of modified starch microencapsulated EO's was conducted by headspace-solid-phase microextraction (HS-SPME). The antimicrobial activity of free and microencapsulated EO's was eva...

since solid-phase and liquid-phase microextraction (spme and lpme) were introduced, as effective solvent-free methods, many efforts have been made to improve their modes and applications. however, due to limitations with sensitivity and efficiency, researchers have focused on improving the performance of their basic primary modes. in this way, in recent years, different methods such as ultrason...

The determination of γ-nonalactone as one of the important odor-active compounds in freshly cooked non-scented rice is reported. It was evaluated by gas chromatography-olfactometry (GC-O) analysis and identified by gas chromatography-mass spectrometry (GC-MS) analysis in the headspace above the freshly cooked non-scented rice samples extracted by using a modified headspace solid-phase microextr...

a headspace-solid phase microextraction (hs-spme) and gas chromatography-mass spectrometry (gc-ms) method has been developed for the simultaneously determination of 20 disinfection by-products (dbps) in water samples from reverse osmosis (ro) membranes. selected compounds belong to different families including: trihalomethanes (thms), halogenated acetonitriles (hans), halogenated nitromethanes ...

In this study the volatile composition of six samples dark chocolates varying in cocoa roasting time (30.5, 34.5 and 38.5 min) geographical origin (Ecuador Ghana) was characterized by headspace solid-phase microextraction (HS-SPME) followed gas chromatography-mass spectrometry (GC-MS). One hundred twenty-one different compounds were identified using a carboxen/polydimethylsiloxane (CAR-PDMS) fi...

The state of the art of analytical procedures based on solid-phase microextraction (SPME) and its applications to tin, mercury, arsenic, antimony, chromium, selenium, and lead determination in abiotic and biotic matrixes are critically reviewed from 1994 to present. First, sample pretreatment prior to SPME is evaluated, including a description of the most usual leaching procedures for sediment,...