A simple and efficient homogenous liquid-liquid extraction method performed in a narrow tube combined with dispersive liquid-liquid microextraction method has been presented for the simultaneous determination of two antiepileptic drugs in urine followed by gas chromatography with flame ionization detection. In this method, a mixture of acetonitrile and urine sample (homogenous solution) is load...

The dependence of the carrier-envelope (CE) phase of the pulses from a hollow-core fiber on the input laser energy was studied using two f-to- 2f interferometers. The CE phase in the in-loop f-to-2f interferometer was measured with the octave spanning white-light spectrum from the hollow-core fiber, whereas the out-of-loop interferometer was based on a sapphire plate. By modulating the input po...

In this study, polyphenylsulfone (PPSU) hollow fiber membrane was fabricated via a wet spinning method with the addition of ethylene glycol (EG) in the range of 0-10 wt% as the additive. The EG was added to improve the membrane pore formation and interconnectivity for better membrane contactor performance in extracting and removing the free fatty acid (FFA) from crude palm oil (CPO). Four diffe...

In this work, the use of a hydrophobic natural deep eutectic solvent (NADES) as supported liquid membrane (SLM) for hollow fiber liquid-phase microextraction (HF-LPME) sulfonamides is proposed. Different NADES based on l-menthol and naturally occurring organic acids (citric acid, formic acetic decanoic nonanoic lactic valeric isobutyric hexanoic octanoic 2-methylbutyric acid) were prepared at d...

Since solid-phase and liquid-phase microextraction (SPME and LPME) were introduced, as effective solvent-free methods, many efforts have been made to improve their modes and applications. However, due to limitations with sensitivity and efficiency, researchers have focused on improving the performance of their basic primary modes. In this way, in recent years, different methods such as ultrason...

The present research describes the use of directly suspended drop microextraction and air-assisted dispersive liquid-liquid microextraction method coupled with UV-Vis spectrophotometer for the analysis of doxepin in water and biological samples. Several important parameters which influence the extraction efficiencies of these two microextraction methods, such as the kind of extracting solven...